(1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-α-D-glucopyranosyl)-4-O-(6''-azido-6''-deoxy-2'',3'',4''-tri-O-benzyl-α-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol

Base Information

Chemical Name:(1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-α-D-glucopyranosyl)-4-O-(6''-azido-6''-deoxy-2'',3'',4''-tri-O-benzyl-α-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol
CAS No.:864862-05-5
Molecular Formula:C₆₀H₆₄N₁₂O₁₀
Molecular Weight:1113.24
Hs Code.:

(1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-α-D-glucopyranosyl)-4-O-(6''-azido-6''-deoxy-2'',3'',4''-tri-O-benzyl-α-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol

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Suppliers and Price of (1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-α-D-glucopyranosyl)-4-O-(6''-azido-6''-deoxy-2'',3'',4''-tri-O-benzyl-α-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol

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Chemical Property of (1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-α-D-glucopyranosyl)-4-O-(6''-azido-6''-deoxy-2'',3'',4''-tri-O-benzyl-α-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol

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Technology Process of (1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-α-D-glucopyranosyl)-4-O-(6''-azido-6''-deoxy-2'',3'',4''-tri-O-benzyl-α-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol

There total 1 articles about (1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-α-D-glucopyranosyl)-4-O-(6''-azido-6''-deoxy-2'',3'',4''-tri-O-benzyl-α-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 864862-02-2
(1S,2S,4S,5S)-2,5-diazidocyclohexane-1,4-diol

: 236115-70-1
6-azido-6-deoxy-2,3,4-tri-O-benzyl-1-phenylthio-β-D-glucopyranoside

: (1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-β-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol

: (1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-α-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol

: (1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-β-D-glucopyranosyl)-4-O-(6''-azido-6''-deoxy-2'',3'',4''-tri-O-benzyl-α-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol

: 864862-05-5
(1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-α-D-glucopyranosyl)-4-O-(6''-azido-6''-deoxy-2'',3'',4''-tri-O-benzyl-α-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol

Guidance literature:: With N-iodo-succinimide; 4 A molecular sieve; silver trifluoromethanesulfonate; In diethyl ether; dichloromethane; at 0 ℃; for 3h; Further byproducts given;
DOI:10.1039/b505865a

Reference yield:

: 864862-05-5
(1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-α-D-glucopyranosyl)-4-O-(6''-azido-6''-deoxy-2'',3'',4''-tri-O-benzyl-α-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol

: (1S,2S,4S,5S)-2,5-Bis-((2S,3R,4S,5R,6R)-6-aminomethyl-3,4,5-tris-benzyloxy-tetrahydro-pyran-2-yloxy)-cyclohexane-1,4-diamine

Guidance literature:: With hydrogen; palladium dihydroxide; In methanol; ethyl acetate; for 48h; atmospheric pressure;
DOI:10.1039/b505865a

Reference yield:

: 864862-05-5
(1S,2S,4S,5S)-1-O-(6'-azido-6'-deoxy-2',3',4'-tri-O-benzyl-α-D-glucopyranosyl)-4-O-(6''-azido-6''-deoxy-2'',3'',4''-tri-O-benzyl-α-D-glucopyranosyl)-2,5-diazido-cyclohexane-1,4-diol

: (1S,2S,4S,5S)-1-O-(6'-amino-6'-deoxy-2',3',4'-triol-α-D-glucopyranosyl)-4-O-(6''-amino-6''-deoxy-2'',3'',4''-triol-α-D-glucopyranosyl)-2,5-diamino-cyclohexane-1,4-diol tetra-acetate salt

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd(OH)2/C / aq. methanol; ethyl acetate / 48 h / atmospheric pressure

2: 77.0 mg / H₂ / Pd(OH)2/C / H₂O / 48 h / atmospheric pressure

With hydrogen; palladium dihydroxide; In methanol; water; ethyl acetate;
DOI:10.1039/b505865a