(Sn(o-C₆H₄PPh₂NSiMe₃)2)

Base Information

• Chemical Name: (Sn(o-C₆H₄PPh₂NSiMe₃)2)
• CAS No.: 293736-64-8
• Molecular Formula: C₄₂H₄₆N₂P₂Si₂Sn
• Molecular Weight: 815.669
• Mol file: 293736-64-8.mol

Synonyms:

Chemical Property of (Sn(o-C₆H₄PPh₂NSiMe₃)2)

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of (Sn(o-C₆H₄PPh₂NSiMe₃)2)

There total 1 articles about (Sn(o-C₆H₄PPh₂NSiMe₃)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

(Li(o-C6H4PPh2NSiMe3))2*Et2O (170958-73-3) + tin(ll) chloride → (Sn(o-C6H4PPh2NSiMe3)2) (293736-64-8)

Guidance literature:

In diethyl ether; byproducts: LiCl; under N2 atm. mixt. (Li(o-C6H4PPh2NSiMe3))2*Et2O and SnCl2 was dissolved in Et2O at -30°C and stirred for 1 day at room temp.; solvent was removed in vac., toluene was added, LiCl was filtered off, soln. was stored at room temp. for 3 days; elem. anal.;

DOI:10.1021/om0003988

upstream raw materials:

(Li(o-C₆H₄PPh₂NSiMe₃))2*Et₂O