[Ru2(CO)2(PPh3)(μ1η(2)-CH2PPh2)(μ-O2CMe)(μ-DPPM)(μ-PPh2)][BPh4]

Base Information

Chemical Name:[Ru2(CO)2(PPh3)(μ1η(2)-CH2PPh2)(μ-O2CMe)(μ-DPPM)(μ-PPh2)][BPh4]
CAS No.:185529-15-1
Molecular Formula:C₂₄H₂₀B*C₇₂H₆₂O₄P₅Ru₂
Molecular Weight:1667.52
Hs Code.:

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Chemical Property of [Ru2(CO)2(PPh3)(μ1η(2)-CH2PPh2)(μ-O2CMe)(μ-DPPM)(μ-PPh2)][BPh4]

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Technology Process of [Ru2(CO)2(PPh3)(μ1η(2)-CH2PPh2)(μ-O2CMe)(μ-DPPM)(μ-PPh2)][BPh4]

There total 1 articles about [Ru2(CO)2(PPh3)(μ1η(2)-CH2PPh2)(μ-O2CMe)(μ-DPPM)(μ-PPh2)][BPh4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 185435-64-7
[Ru2(CO)2(MeCN)2(μ-O2CMe)(μ-DPPM)2][BPh4]

: 143-66-8
sodium tetraphenyl borate

: 603-35-0
triphenylphosphine

: [Ru2(CO)2(PPh3)2(μ-O2CMe)(μ-DPPM)(μ-PPh2)]

: 185435-68-1,185529-15-1
[Ru2(CO)2(PPh3)(μ1η(2)-CH2PPh2)(μ-O2CMe)(μ-DPPM)(μ-PPh2)][BPh4]

Guidance literature:: In acetonitrile; inert atmosphere; refluxing of soln. of PPh3 and Ru-compd. (equiv. amts., 7 h), filtration off minor product (washing (ACN), drying (vac.)); addn. of NaBPh4 to filtrate, stirring (0.5 h),; evapn. (vac.), recrystn. (CH2Cl2/MeOH), washing (ACN), drying (vac.); elem. anal.; isolated as mixture of two isomers;
DOI:10.1021/om960572l