di(2,4,6-trichlorophenolato)triphenylantimony(V)

Base Information

• Chemical Name: di(2,4,6-trichlorophenolato)triphenylantimony(V)
• CAS No.: 102086-70-4
• Molecular Formula: C₃₀H₁₉Cl₆O₂Sb
• Molecular Weight: 745.948
• Mol file: 102086-70-4.mol

Synonyms:

Chemical Property of di(2,4,6-trichlorophenolato)triphenylantimony(V)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of di(2,4,6-trichlorophenolato)triphenylantimony(V)

There total 2 articles about di(2,4,6-trichlorophenolato)triphenylantimony(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.4%

triphenylantimony dibromide (1538-59-6,20265-30-9,34716-92-2) + 2,4,6-Trichlorophenol (88-06-2,67471-29-8) → di(2,4,6-trichlorophenolato)triphenylantimony(V) (102086-70-4)

Guidance literature:

With triethylamine; In benzene; byproducts: Et3NHBr; 2 equiv. Cl3C6H2OH and Et3N are stirred in dry benzene at 25-30 °C for about 1 h, refluxed for 2 h; Et3NHCl was filtered off, the filtrate was concd., petroleum ether was added, recrystd. (benzene/petroleum ether); elem. anal.;

Reference yield: 65.6%

triphenylantimony dibromide (1538-59-6,20265-30-9,34716-92-2) + sodium 2,4,6-trichlorophenolate (3784-03-0) → di(2,4,6-trichlorophenolato)triphenylantimony(V) (102086-70-4)

Guidance literature:

In benzene; byproducts: NaBr; 2 equiv. Cl3C6H2ONa are refluxed for about 4 h; NaBr was filtered off, the filtrate was concd., petroleum ether was added, recrystd. (benzene/petroleum ether); elem. anal.;

upstream raw materials:

triphenylantimony dibromide

2,4,6-Trichlorophenol

sodium 2,4,6-trichlorophenolate