5-(Trifluoromethyl)-1H-indole-3-carboxaldehyde

Base Information

• Chemical Name: 5-(Trifluoromethyl)-1H-indole-3-carboxaldehyde
• CAS No.: 468718-16-3
• Molecular Formula: C10H6F3NO
• Molecular Weight: 213.16
• Hs Code.: 2933998090
• Mol file: 468718-16-3.mol

Synonyms:5-(Trifuoromethyl)-1H-indol-3-carbaldehyde;5-(Trifluoromethyl)-1H-indole-3-carbaldehyde;5-(Trifluoromethyl)-1H-indole-3-carboxaldehyde;1H-Indole-3-carboxaldehyde, 5-(trifluoromethyl)-

Chemical Property of 5-(Trifluoromethyl)-1H-indole-3-carboxaldehyde

Chemical Property:

• Boiling Point: 333.508 °C at 760 mmHg
• Flash Point: 155.5 °C
• Density: 1.45 g/cm³

Purity/Quality:

97% ^*data from raw suppliers

5-(Trifluoromethyl)-1H-indole-3-carbaldehyde 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-(Trifluoromethyl)-1H-indole-3-carboxaldehyde

There total 4 articles about 5-(Trifluoromethyl)-1H-indole-3-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethyl-formamide (68-12-2,33513-42-7) + 5-trifluoromethyl-1H-indole (100846-24-0) → 5-(trifluoromethyl)-1H-indole-3-carbaldehyde (468718-16-3)

Guidance literature:

N,N-dimethyl-formamide; With trichlorophosphate; at 5 - 20 ℃; for 0.833333h;

5-trifluoromethyl-1H-indole; at 5 - 60 ℃; for 1.83333h;

Reference yield:

p-nitrobenzotrifluoride (402-54-0) → 5-(trifluoromethyl)-1H-indole-3-carbaldehyde (468718-16-3)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride; potassium tert-butylate / N,N-dimethyl-formamide

2: palladium-carbon / ethanol; water; acetic acid

With hydrogenchloride; potassium tert-butylate; palladium-carbon; In ethanol; water; acetic acid; N,N-dimethyl-formamide;

Reference yield:

5-trifluoromethyl-1H-indole (100846-24-0) → 5-(trifluoromethyl)-1H-indole-3-carbaldehyde (468718-16-3)

Guidance literature:

upstream raw materials:

N,N-dimethyl-formamide

5-trifluoromethyl-1H-indole

2-(2-nitro-5-(trifluoromethyl)phenyl)acetonitrile

p-nitrobenzotrifluoride

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