4,9-bis{[3,5-bis(1,1-dimethylethyl)phenyl]amino}-2,7-bis{4-[(1,1-dimethylethyl)sulfanyl]phenyl}benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone

Base Information

Chemical Name:4,9-bis{[3,5-bis(1,1-dimethylethyl)phenyl]amino}-2,7-bis{4-[(1,1-dimethylethyl)sulfanyl]phenyl}benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone
CAS No.:916503-44-1
Molecular Formula:C₆₂H₇₂N₄O₄S₂
Molecular Weight:1001.41
Hs Code.:

4,9-bis{[3,5-bis(1,1-dimethylethyl)phenyl]amino}-2,7-bis{4-[(1,1-dimethylethyl)sulfanyl]phenyl}benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone

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Chemical Property of 4,9-bis{[3,5-bis(1,1-dimethylethyl)phenyl]amino}-2,7-bis{4-[(1,1-dimethylethyl)sulfanyl]phenyl}benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone

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Technology Process of 4,9-bis{[3,5-bis(1,1-dimethylethyl)phenyl]amino}-2,7-bis{4-[(1,1-dimethylethyl)sulfanyl]phenyl}benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone

There total 4 articles about 4,9-bis{[3,5-bis(1,1-dimethylethyl)phenyl]amino}-2,7-bis{4-[(1,1-dimethylethyl)sulfanyl]phenyl}benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 916503-43-0
4,9-dichloro-2,7-bis{4-[(1,1-dimethylethyl)sulfanyl]phenyl}benzo[lmn][3,8]phenanthroline-1,3,6,8-(2H,7H)-tetrone

: 2380-36-1
3,5-di-tert-butylaniline

: 916503-44-1
4,9-bis{[3,5-bis(1,1-dimethylethyl)phenyl]amino}-2,7-bis{4-[(1,1-dimethylethyl)sulfanyl]phenyl}benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone

Guidance literature:: In N,N-dimethyl-formamide; at 120 ℃; for 16h;
DOI:10.1002/hlca.200690190

Reference yield:

: 7205-66-5
1-(1,1-dimethylethyl)sulfanyl-4-nitrobenzene

: 916503-44-1
4,9-bis{[3,5-bis(1,1-dimethylethyl)phenyl]amino}-2,7-bis{4-[(1,1-dimethylethyl)sulfanyl]phenyl}benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Sn; HCl / ethanol / 1 h / 20 °C

2: 67 percent / acetic acid / 0.5 h / 110 °C

3: 70 percent / dimethylformamide / 16 h / 120 °C

With hydrogenchloride; tin; In ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/hlca.200690190

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 916503-44-1
4,9-bis{[3,5-bis(1,1-dimethylethyl)phenyl]amino}-2,7-bis{4-[(1,1-dimethylethyl)sulfanyl]phenyl}benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / dimethylformamide / 1 h / 20 °C

2: 95 percent / Sn; HCl / ethanol / 1 h / 20 °C

3: 67 percent / acetic acid / 0.5 h / 110 °C

4: 70 percent / dimethylformamide / 16 h / 120 °C

With hydrogenchloride; tin; In ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/hlca.200690190