4-chloro-N-(2-methoxybenzylidene)aniline

Base Information

• Chemical Name: 4-chloro-N-(2-methoxybenzylidene)aniline
• CAS No.: 24588-83-8
• Molecular Formula: C14H12ClNO
• Molecular Weight: 245.708
• European Community (EC) Number: 667-276-8
• DSSTox Substance ID: DTXSID40359463
• Mol file: 24588-83-8.mol

Synonyms:AGN-PC-0JYNII;DTXSID40359463;AKOS003623443;24588-83-8;4-chloro-N-(2-methoxybenzylidene)aniline

Chemical Property of 4-chloro-N-(2-methoxybenzylidene)aniline

Chemical Property:

• XLogP3: 4.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 245.0607417
• Heavy Atom Count: 17
• Complexity: 249

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=CC=C1C=NC2=CC=C(C=C2)Cl

Technology Process of 4-chloro-N-(2-methoxybenzylidene)aniline

There total 1 articles about 4-chloro-N-(2-methoxybenzylidene)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

4-chloro-aniline (106-47-8) + ortho-anisaldehyde (135-02-4) → 4-chloro-N-(2-methoxy-benzylidene)-aniline (24588-83-8)

Guidance literature:

In ethanol; for 2h; Reflux;

DOI:10.1016/j.bioorg.2016.10.007

Reference yield: 35.0%

4-chloro-N-(2-methoxy-benzylidene)-aniline (24588-83-8) + phosphonic acid diethyl ester (762-04-9) → diethyl (4-chlorophenylamino)(2-methoxyphenyl)methylphosphonate

Guidance literature:

In ethanol; Reflux;

DOI:10.1016/j.bioorg.2016.10.007

Reference yield: 31.4%

2,5-dimethylpyridine (589-93-5) + 4-chloro-N-(2-methoxy-benzylidene)-aniline (24588-83-8) → 2,5-Bis-[(E)-2-(2-methoxy-phenyl)-vinyl]-pyridine

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; at 90 - 95 ℃; for 1h;

DOI:10.1002/hlca.19800630524

upstream raw materials:

4-chloro-aniline

ortho-anisaldehyde

Downstream raw materials:

2-[4-(2-methoxy-styryl)-phenyl]-2H-[1,3]dioxolo[4',5':4,5]benzo[1,2-d][1,2,3]triazole

(4-Chloro-phenyl)-[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-amine; compound with trichloro-acetic acid

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