1-(2-Methoxyphenyliminomethyl)-2-naphthol

Base Information

• Chemical Name: 1-(2-Methoxyphenyliminomethyl)-2-naphthol
• CAS No.: 20772-78-5
• Molecular Formula: C₁₈H₁₅NO₂
• Molecular Weight: 277.323
• European Community (EC) Number: 665-447-1
• DSSTox Substance ID: DTXSID00425178
• Nikkaji Number: J705.142E
• Mol file: 20772-78-5.mol

Synonyms:20772-78-5;1-(((2-Methoxyphenyl)imino)methyl)naphthalen-2-ol;1-(2-METHOXYPHENYLIMINOMETHYL)-2-NAPHTHOL;DTXSID00425178;MFCD00029278;AKOS003671509;1-[(2-Methoxy-phenylimino)-methyl]-naphthalen-2-ol;1-((e)-(2-methoxyphenylimino) methyl)naphthalene-2-ol;1-[(2-Methoxyanilino)methylidene]naphthalen-2(1H)-one;1-[(E)-[(2-methoxyphenyl)imino]methyl]naphthalen-2-ol

Chemical Property of 1-(2-Methoxyphenyliminomethyl)-2-naphthol

Chemical Property:

• XLogP3: 4.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 277.110278721
• Heavy Atom Count: 21
• Complexity: 357

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=CC=C1N=CC2=C(C=CC3=CC=CC=C32)O

Technology Process of 1-(2-Methoxyphenyliminomethyl)-2-naphthol

There total 2 articles about 1-(2-Methoxyphenyliminomethyl)-2-naphthol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.5%

2-methoxy-phenylamine (90-04-0) + 2-hydroxynaphthalene-1-carbaldehyde (708-06-5) → 1-((2′-methoxylphenylimino)methyl)naphthalen-2-ol (20772-78-5)

Guidance literature:

In ethanol; for 1h; Heating;

DOI:10.1107/S0108270105018044

Reference yield:

2-methoxy-phenylamine (90-04-0) + 2-hydroxynaphthalene-1-carbaldehyde (708-06-5) → 1<(2'-methoxyphenylimino)methyl>-2-naphthol (20772-78-5)

Guidance literature:

With hydrogenchloride; In ethanol;

DOI:10.1016/0040-4020(68)88164-5

Reference yield:

uranyl chloride + 1-((2′-methoxylphenylimino)methyl)naphthalen-2-ol (20772-78-5) → UO2(2+)*2Cl(1-)*2C18H15NO2=UO2Cl2*2C18H15NO2

Guidance literature:

In ethanol; refluxing;

DOI:10.1007/BF00912795

upstream raw materials:

2-methoxy-phenylamine

2-hydroxynaphthalene-1-carbaldehyde

Downstream raw materials:

bis[1-[(2'-OMe-phenylimino)methyl]-2-naphtholato]cobalt(II) complex