lithium tetrakis(1-cyclohexyltetrazol-5-ato)aurate(III)

Base Information

Chemical Name:lithium tetrakis(1-cyclohexyltetrazol-5-ato)aurate(III)
CAS No.:220205-44-7
Molecular Formula:C₂₈H₄₄AuN₁₆*Li
Molecular Weight:808.672
Hs Code.:

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Chemical Property of lithium tetrakis(1-cyclohexyltetrazol-5-ato)aurate(III)

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Technology Process of lithium tetrakis(1-cyclohexyltetrazol-5-ato)aurate(III)

There total 1 articles about lithium tetrakis(1-cyclohexyltetrazol-5-ato)aurate(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 19597-69-4,157302-05-1
lithium azide

: 13682-61-6
potassium tetrachloroaurate(III)

: 931-53-3
Cyclohexyl isocyanide

: 220205-44-7
lithium tetrakis(1-cyclohexyltetrazol-5-ato)aurate(III)

Guidance literature:: In ethanol; addn. dropwise of soln. of K(AuCl4) in EtOH to soln. of LiN3 in EtOH, stirring for 1 h, addn. of cyclohexyl isocyanide; addn. of water, conc. in vac., cooling to 0°C, pptn., filtration,washing with cold water, drying in high vac., elem. anal.;
DOI:10.1016/S0022-328X(00)00457-5

Reference yield: 95.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 220205-44-7
lithium tetrakis(1-cyclohexyltetrazol-5-ato)aurate(III)

: tris(1-cyclohexyl-tetrazol-5-ato)(1-cyclohexyl-tetrazol-5-ylidene)gold(III)

Guidance literature:: In water; dissolving of Na(Au(CN4C6H11)4) in warm water, dropwise addn. of dilutedhydrochloric acid; pptn., washing with water, recrystn. from ethanol-water, elem. anal.;
DOI:10.1016/S0022-328X(00)00457-5