dimethyl (1R,2S,5R*)-5-methyl-cyclohexane-1,2-dicarboxylate

Base Information

Chemical Name:dimethyl (1R*,2S*,5R*)-5-methyl-cyclohexane-1,2-dicarboxylate
CAS No.:19491-57-7
Molecular Formula:C₁₁H₁₈O₄
Molecular Weight:214.262
Hs Code.:

Synonyms:

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Chemical Property of dimethyl (1R*,2S*,5R*)-5-methyl-cyclohexane-1,2-dicarboxylate

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Technology Process of dimethyl (1R*,2S*,5R*)-5-methyl-cyclohexane-1,2-dicarboxylate

There total 5 articles about dimethyl (1R*,2S*,5R*)-5-methyl-cyclohexane-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1694-82-2
cis-3a,4,7,7a-tetrahydro-5-methyl-1,3-isobenzofurandione

: 19491-57-7,19491-58-8,19491-59-9,19491-60-2,92709-07-4
dimethyl (1R*,2S*,5R*)-5-methyl-cyclohexane-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethyl acetate

2: CF₃CO₂H

With hydrogen; palladium on activated charcoal; trifluoroacetic acid; In ethyl acetate;
DOI:10.1016/S0040-4020(01)90572-1

Reference yield:

: 106542-15-8,106552-44-7
5-methyl-2-ethenylcyclohexanecarboxylic acid

: 19491-57-7,19491-58-8,19491-59-9,19491-60-2,92709-07-4
dimethyl (1R*,2S*,5R*)-5-methyl-cyclohexane-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: RuO₄

2: diethyl ether

With ruthenium tetroxide; In diethyl ether;
DOI:10.1016/S0040-4020(01)90572-1

Reference yield:

: 106540-63-0
(Z)-9-hydroxy-4-methyl-7-nonenoic acid

: 19491-57-7,19491-58-8,19491-59-9,19491-60-2,92709-07-4
dimethyl (1R*,2S*,5R*)-5-methyl-cyclohexane-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 15 percent / 2-chloro-1-methylpyridinium iodide / acetonitrile / 4 h / Heating

2: 1.) LDA; t-BuMe₂SiCl; 2.) HF / 2.) -30 deg C, 2h; 2.) CH₃CN

3: RuO₄

4: diethyl ether

With ruthenium tetroxide; hydrogen fluoride; 2-chloro-1-methyl-pyridinium iodide; tert-butyldimethylsilyl chloride; lithium diisopropyl amide; In diethyl ether; acetonitrile;
DOI:10.1016/S0040-4020(01)90572-1