2-bromo-1,2,3,4-tetrahydrotetraphen-1-yl {[(1S,2R,5S)-5-methyl-2-(propan-2-yl)cyclohexyl]oxy}acetate

Base Information

Chemical Name:2-bromo-1,2,3,4-tetrahydrotetraphen-1-yl {[(1S,2R,5S)-5-methyl-2-(propan-2-yl)cyclohexyl]oxy}acetate
CAS No.:91050-74-7
Molecular Formula:C₃₀H₃₅BrO₃
Molecular Weight:523.51
Hs Code.:

Synonyms:

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Chemical Property of 2-bromo-1,2,3,4-tetrahydrotetraphen-1-yl {[(1S,2R,5S)-5-methyl-2-(propan-2-yl)cyclohexyl]oxy}acetate

Chemical Property:

Vapor Pressure:1.89E-16mmHg at 25°C

Purity/Quality:

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Technology Process of 2-bromo-1,2,3,4-tetrahydrotetraphen-1-yl {[(1S,2R,5S)-5-methyl-2-(propan-2-yl)cyclohexyl]oxy}acetate

There total 5 articles about 2-bromo-1,2,3,4-tetrahydrotetraphen-1-yl {[(1S,2R,5S)-5-methyl-2-(propan-2-yl)cyclohexyl]oxy}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57652-74-1
3,4-dihydrobenz anthracen-1(2H)-one

: 91050-74-7
(+)-(1S,2S)-trans-2-bromo-1-menthyloxyacetoxy-1,2,3,4-tetrahydrobenz anthracene

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / sodium borohydride / methanol / 4 h / Ambient temperature

2: 74 percent / toluene-p-sulphonic acid / benzene / 0.5 h / Heating

3: 62 percent / lithium acetate, / acetic acid / 0.75 h / Ambient temperature

4: 75 percent / diborane / tetrahydrofuran

5: pyridine

With sodium tetrahydroborate; lithium acetate; toluene-4-sulfonic acid; diborane; In tetrahydrofuran; pyridine; methanol; acetic acid; benzene;
DOI:10.1039/P19840000839

Reference yield:

: 60968-00-5
(+/-)-1-hydroxy-1,2,3,4-tetrahydrobenz anthracene

: 91050-74-7
(+)-(1S,2S)-trans-2-bromo-1-menthyloxyacetoxy-1,2,3,4-tetrahydrobenz anthracene

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / toluene-p-sulphonic acid / benzene / 0.5 h / Heating

2: 62 percent / lithium acetate, / acetic acid / 0.75 h / Ambient temperature

3: 75 percent / diborane / tetrahydrofuran

4: pyridine

With lithium acetate; toluene-4-sulfonic acid; diborane; In tetrahydrofuran; pyridine; acetic acid; benzene;
DOI:10.1039/P19840000839

Reference yield:

: 60968-01-6
3,4-Dihydrobenz anthracene

: 91050-74-7
(+)-(1S,2S)-trans-2-bromo-1-menthyloxyacetoxy-1,2,3,4-tetrahydrobenz anthracene

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / lithium acetate, / acetic acid / 0.75 h / Ambient temperature

2: 75 percent / diborane / tetrahydrofuran

3: pyridine

With lithium acetate; diborane; In tetrahydrofuran; pyridine; acetic acid;
DOI:10.1039/P19840000839