[Pt((2,7-di-tert-butylfluoren-9-ylidene)methanedithiolato)2(Au(PCy₃))2]

Base Information

• Chemical Name: [Pt((2,7-di-tert-butylfluoren-9-ylidene)methanedithiolato)2(Au(PCy₃))2]
• CAS No.: 939785-15-6
• Molecular Formula: C₈₀H₁₁₄Au₂P₂PtS₄
• Molecular Weight: 1855.01

Synonyms:

Chemical Property of [Pt((2,7-di-tert-butylfluoren-9-ylidene)methanedithiolato)2(Au(PCy₃))2]

Chemical Property:

Purity/Quality:

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Technology Process of [Pt((2,7-di-tert-butylfluoren-9-ylidene)methanedithiolato)2(Au(PCy₃))2]

There total 1 articles about [Pt((2,7-di-tert-butylfluoren-9-ylidene)methanedithiolato)2(Au(PCy₃))2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

(tricyclohexylphosphine)gold(I) chloride (49763-41-9) + (Pr4N)2[Pt((2,7-di-tert-butylfluoren-9-ylidene)methanedithiolato)2] + silver perchlorate → [Pt((2,7-di-tert-butylfluoren-9-ylidene)methanedithiolato)2(Au(PCy3))2] (939785-15-6)

Guidance literature:

In acetone; byproducts: AgCl; AgClO4 was added to a stirred suspn. of AuClP(C6H11)3 in acetone, after 10 min the mixt. was filtered (AgCl), Pt-complex was added to the filtrate, the mixt. was stirred for 30 min; ppt. was filtered off, washed with acetone, recrystd. from CH2Cl2-diethyl ether, vac.-dried; elem. anal.;

DOI:10.1021/ic070164h

upstream raw materials:

(tricyclohexylphosphine)gold(I) chloride

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