RuH(κ3N-1,3-di(2-pyridyl)-2-azaallyl)(PPh3)2

Base Information

Chemical Name:RuH(κ3N-1,3-di(2-pyridyl)-2-azaallyl)(PPh3)2
CAS No.:1338603-10-3
Molecular Formula:C₄₈H₄₁N₃P₂Ru
Molecular Weight:822.891
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of RuH(κ3N-1,3-di(2-pyridyl)-2-azaallyl)(PPh3)2

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Technology Process of RuH(κ3N-1,3-di(2-pyridyl)-2-azaallyl)(PPh3)2

There total 2 articles about RuH(κ3N-1,3-di(2-pyridyl)-2-azaallyl)(PPh3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1338603-08-9
[RuH[κ3N-fac-1,3-di(2-pyridylmethyl)amine](PPh3)2]Cl

: 865-47-4
potassium tert-butylate

: 1338603-10-3
RuH(κ3N-1,3-di(2-pyridyl)-2-azaallyl)(PPh3)2

Guidance literature:: In tetrahydrofuran; byproducts: H2; (under Ar, Schlenk); suspn. of Ru-complex in THF placed in vial, KOC(CH3)3 in THF added, heated at 60°C overnight; filtered, dried in vacuo, pentane added, stirred for 1 h, filtered, solvent removed in vacuo; elem. anal.;
DOI:10.1039/c1dt10626k