salicylaldehyde morpholine N-thiohydrazone

Base Information

Chemical Name:salicylaldehyde morpholine N-thiohydrazone
CAS No.:60033-78-5
Molecular Formula:C₁₂H₁₅N₃O₂S
Molecular Weight:265.336
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of salicylaldehyde morpholine N-thiohydrazone

Chemical Property:

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Technology Process of salicylaldehyde morpholine N-thiohydrazone

There total 2 articles about salicylaldehyde morpholine N-thiohydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6499-15-6
4-morpholinothiosemicarbazide

: 90-02-8
salicylaldehyde

: 60033-78-5
salicylaldehyde morpholine-N-thiohydrazone

Guidance literature:: In ethanol; for 2h; Heating;

Reference yield:

: 862873-20-9
4-(1H-imidazol-1-ylcarbonothioyl)morpholine

: 60033-78-5
salicylaldehyde morpholine-N-thiohydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 3 h / 20 °C / Reflux

2: acetic acid / ethanol / 0.5 h / 83 °C / Microwave irradiation

With hydrazine hydrate; acetic acid; In ethanol; 2: |Schiff Reaction;
DOI:10.1371/journal.pone.0110291

Reference yield: 70.0%

: chromium chloride hexahydrate

: 60033-78-5
salicylaldehyde morpholine-N-thiohydrazone

: Cr⁽³⁺⁾*2Cl^(1-)*(OC₆H₄CHNNHCSNC₄H₈O)^(1-)*6H₂O=[CrCl₂(H₂O)(OC₆H₄CHNNHCSNC₄H₈O)]*5H₂O

Guidance literature:: With NaCH₃COO; In ethanol; addn. of hot soln. of CrCl3*6H2O (1 equiv.) in ethanol to hot soln. of salicylaldehyde morpholine N-thiohydrazone ( 1 equiv.) in ethanol, immediate addn. of anhyd. NaCH3COO in hot ethanol (pH 5); reflux for 2 h; hot filtration, washing with water and cold ethanol, drying in vac.; elem. anal.;