C₃₉H₂₂F₈

Base Information

Chemical Name:C₃₉H₂₂F₈
CAS No.:1259293-46-3
Molecular Formula:C₃₉H₂₂F₈
Molecular Weight:642.591
Hs Code.:

C<sub>39</sub>H<sub>22</sub>F<sub>8</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₉H₂₂F₈

Chemical Property:

Purity/Quality:

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Technology Process of C₃₉H₂₂F₈

There total 5 articles about C₃₉H₂₂F₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86-73-7
9H-fluorene

: 1259293-46-3
C₃₉H₂₂F₈

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide / 1,2-propylene cyclic carbonate / 3 h / Reflux

2: chromium(VI) oxide; acetic acid / 1 h / 120 °C

3: iodine; magnesium / diethyl ether

4: trifluorormethanesulfonic acid

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; toluene

With chromium(VI) oxide; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trifluorormethanesulfonic acid; iodine; sodium carbonate; magnesium; acetic acid; In 1,2-propylene cyclic carbonate; diethyl ether; water; toluene; 3: Grignard reaction / 5: Suzuki coupling;
DOI:10.1021/ma102093t

Reference yield:

: 16433-88-8
2,7-dibromo-9H-fluorene

: 1259293-46-3
C₃₉H₂₂F₈

Guidance literature:: Multi-step reaction with 4 steps

1: chromium(VI) oxide; acetic acid / 1 h / 120 °C

2: iodine; magnesium / diethyl ether

3: trifluorormethanesulfonic acid

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; toluene

With chromium(VI) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trifluorormethanesulfonic acid; iodine; sodium carbonate; magnesium; acetic acid; In diethyl ether; water; toluene; 2: Grignard reaction / 4: Suzuki coupling;
DOI:10.1021/ma102093t

Reference yield:

: 393-37-3
5-bromo-2-fluorobenzotrifluoride

: 1259293-46-3
C₃₉H₂₂F₈

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; magnesium / tetrahydrofuran; diethyl ether

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; toluene

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; iodine; sodium carbonate; magnesium; In tetrahydrofuran; diethyl ether; water; toluene; 1: Grignard reaction / 1: Grignard reaction / 2: Suzuki coupling;
DOI:10.1021/ma102093t