C₅₉H₉₄O₈Si₃

Base Information

• Chemical Name: C₅₉H₉₄O₈Si₃
• CAS No.: 1322588-82-8
• Molecular Formula: C₅₉H₉₄O₈Si₃
• Molecular Weight: 1015.65
• Mol file: 1322588-82-8.mol

Synonyms:

Chemical Property of C₅₉H₉₄O₈Si₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₉H₉₄O₈Si₃

There total 15 articles about C₅₉H₉₄O₈Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

2-methyl-4H-pyran-4-one (5848-33-9) + C53H88O6Si3 (1322588-79-3) → C59H94O8Si3 (1322588-82-8)

Guidance literature:

With lithium hexamethyldisilazane; at -78 ℃; for 1h;

DOI:10.1080/00397911.2010.516462

Reference yield:

C10H20O3 → C59H94O8Si3 (1322588-82-8)

Guidance literature:

Multi-step reaction with 8 steps

1: potassium hydride / tetrahydrofuran

2: sodium periodate; osmium(VIII) oxide; 4-methylmorpholine N-oxide

3: lithium diisopropyl amide

4: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 22 h / -30 °C

5: 2,6-dimethylpyridine

6: hydrogenchloride / isopropyl alcohol / 6 h / 70 °C

7: oxalyl dichloride; dimethyl sulfoxide

8: lithium hexamethyldisilazane / 1 h / -78 °C

With 2,6-dimethylpyridine; hydrogenchloride; sodium periodate; osmium(VIII) oxide; oxalyl dichloride; potassium hydride; acetic acid; dimethyl sulfoxide; 4-methylmorpholine N-oxide; lithium hexamethyldisilazane; tetramethylammonium triacetoxyborohydride; lithium diisopropyl amide; In tetrahydrofuran; isopropyl alcohol; acetonitrile; 3: Aldol addition / 7: Swern oxidation;

DOI:10.1080/00397911.2010.516462

Reference yield:

C37H54O7Si → C59H94O8Si3 (1322588-82-8)

Guidance literature:

Multi-step reaction with 6 steps

1: toluene-4-sulfonic acid / tetrahydrofuran

2: acetic acid / water

3: 2,6-dimethylpyridine

4: hydrogenchloride / isopropyl alcohol / 6 h / 70 °C

5: oxalyl dichloride; dimethyl sulfoxide

6: lithium hexamethyldisilazane / 1 h / -78 °C

With 2,6-dimethylpyridine; hydrogenchloride; oxalyl dichloride; toluene-4-sulfonic acid; acetic acid; dimethyl sulfoxide; lithium hexamethyldisilazane; In tetrahydrofuran; water; isopropyl alcohol; 5: Swern oxidation;

DOI:10.1080/00397911.2010.516462

upstream raw materials:

C₃₇H₅₄O₇Si

C₄₀H₅₈O₇Si

C₅₅H₉₄O₇Si₃

C₅₃H₉₀O₆Si₃

Downstream raw materials:

C₅₇H₁₀₀O₇Si₄

C₅₇H₁₀₀O₇Si₄

C₆₅H₁₀₈O₈Si₄