Technology Process of C31H45NO2
There total 12 articles about C31H45NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) sodium hydride / 1.) DMF, 10 deg C, 40 min, 2.) a) 10 deg C, 4 h, b) RT, 14 h
2: H2 / 10percent Pd/C / acetic acid / 62 h / 72 °C / 2280 Torr
3: 6 N HCl / 48 h / 110 °C
4: Bio-Rad AG3 * 4A (hydroxide form) / H2O
5: ethanol; tetrahydrofuran / Irradiation
With
hydrogenchloride; Bio-Rad AG3 * 4A (hydroxide form); hydrogen; sodium hydride;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; water; acetic acid;
DOI:10.1021/ja00167a054
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) sodium hydride / 1.) DMF, 10 deg C, 40 min, 2.) a) 10 deg C, 4 h, b) RT, 14 h
2: H2 / 10percent Pd/C / acetic acid / 62 h / 72 °C / 2280 Torr
3: 6 N HCl / 48 h / 110 °C
4: Bio-Rad AG3 * 4A (hydroxide form) / H2O
5: ethanol; tetrahydrofuran / Irradiation
With
hydrogenchloride; Bio-Rad AG3 * 4A (hydroxide form); hydrogen; sodium hydride;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; water; acetic acid;
DOI:10.1021/ja00167a054
- Guidance literature:
-
Multi-step reaction with 4 steps
1: H2 / 10percent Pd/C / acetic acid / 62 h / 72 °C / 2280 Torr
2: 6 N HCl / 48 h / 110 °C
3: Bio-Rad AG3 * 4A (hydroxide form) / H2O
4: ethanol; tetrahydrofuran / Irradiation
With
hydrogenchloride; Bio-Rad AG3 * 4A (hydroxide form); hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; water; acetic acid;
DOI:10.1021/ja00167a054