C₄₁H₄₅ClO₇

Base Information

• Chemical Name: C₄₁H₄₅ClO₇
• CAS No.: 1339957-66-2
• Molecular Formula: C₄₁H₄₅ClO₇
• Molecular Weight: 685.257
• Mol file: 1339957-66-2.mol

Synonyms:

Chemical Property of C₄₁H₄₅ClO₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₁H₄₅ClO₇

There total 11 articles about C₄₁H₄₅ClO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H11ClO5 (1277122-87-8) → C41H45ClO7 (1339957-66-2)

Guidance literature:

Multi-step reaction with 4 steps

1: thionyl chloride

2: pyridine / dichloromethane / 20 h / Reflux

3: ammonium hydroxide / tetrahydrofuran / 20 °C

4: dmap; dicyclohexyl-carbodiimide / dichloromethane

With pyridine; dmap; ammonium hydroxide; thionyl chloride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;

DOI:10.1039/c1jm12131f

Reference yield:

C23H25ClO7 → C41H45ClO7 (1339957-66-2)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium hydroxide / tetrahydrofuran / 20 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane

With dmap; ammonium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;

DOI:10.1039/c1jm12131f

Reference yield:

(2S)-2-methyl-1-butanol (1565-80-6) → C41H45ClO7 (1339957-66-2)

Guidance literature:

Multi-step reaction with 4 steps

1: benzene / 25 h / Reflux

2: pyridine / dichloromethane / 20 h / Reflux

3: ammonium hydroxide / tetrahydrofuran / 20 °C

4: dmap; dicyclohexyl-carbodiimide / dichloromethane

With pyridine; dmap; ammonium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; benzene;

DOI:10.1039/c1jm12131f

upstream raw materials:

C₁₅H₁₁ClO₅

C₂₁H₂₃ClO₅

4-(heptyloxy)-4'-biphenylcarboxylic acid

(S)-2-methylbutyl (S)-lactate