C₂₇H₅₀OSi₂

Base Information

Chemical Name:C₂₇H₅₀OSi₂
CAS No.:1350626-85-5
Molecular Formula:C₂₇H₅₀OSi₂
Molecular Weight:446.864
Hs Code.:

C<sub>27</sub>H<sub>50</sub>OSi<sub>2</sub>

Synonyms:

Suppliers and Price of C₂₇H₅₀OSi₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₅₀OSi₂

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₂₇H₅₀OSi₂

There total 10 articles about C₂₇H₅₀OSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6485-79-6
chlorotriisopropylsilane

: 1266551-69-2
tert-butyldimethyl((6-phenylhex-2-yn-1-yl)oxy)silane

: 1350626-87-7
C₂₇H₅₀OSi₂

: 1350626-85-5
C₂₇H₅₀OSi₂

Guidance literature:: With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In 5,5-dimethyl-1,3-cyclohexadiene; at 80 ℃; for 1h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ja209553f

Reference yield:

: 1172850-67-7
C₁₇H₂₂O₂

: 1350626-85-5
C₂₇H₅₀OSi₂

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C / Inert atmosphere

2: 1H-imidazole / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene / 18 h / Reflux

With 1H-imidazole; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene;
DOI:10.1021/ja209553f

Reference yield:

: 637-59-2
1-Bromo-3-phenylpropane

: 1350626-85-5
C₂₇H₅₀OSi₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / 0 °C / Inert atmosphere

1.2: 5 h / -78 - 20 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C / Inert atmosphere

3.1: 1H-imidazole / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

4.1: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene / 18 h / Reflux

With 1H-imidazole; n-butyllithium; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; hexane;
DOI:10.1021/ja209553f