C₁₅H₂₇B₃O₃

Base Information

• Chemical Name: C₁₅H₂₇B₃O₃
• CAS No.: 1365543-21-0
• Molecular Formula: C₁₅H₂₇B₃O₃
• Molecular Weight: 287.811
• Mol file: 1365543-21-0.mol

Synonyms:

Chemical Property of C₁₅H₂₇B₃O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₅H₂₇B₃O₃

There total 2 articles about C₁₅H₂₇B₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R,R)-hydroxybenzoin (52340-78-0) + cyclopentane boronic acid (63076-51-7) → (4R,5R)-C5H9B(hydrobenzoinate) (1365543-20-9) + C15H27B3O3 (1365543-21-0)

Guidance literature:

In chloroform-d1; for 2h; Molecular sieve; Reflux;

DOI:10.1039/c2ob06872a

Reference yield:

benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) + cyclopentane boronic acid (63076-51-7) → C15H27B3O3 (1365543-21-0) + 2-cyclopentyl-benzo[1,3,2]dioxaborole (32999-14-7)

Guidance literature:

With molecular sieves; In chloroform-d1; byproducts: H2O; addn. of catechol to CDCl3 soln. of boronic acid deriv., refluxing for 2h in presence of molecular sieves; filtration, not isolated, NMR;

DOI:10.1039/c2ob06872a

upstream raw materials:

(R,R)-hydroxybenzoin

cyclopentane boronic acid

benzene-1,2-diol

Refernces