2-{2-[4-(4-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine; compound with (E)-but-2-enedioic acid

Base Information

• Chemical Name: 2-{2-[4-(4-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine; compound with (E)-but-2-enedioic acid
• CAS No.: 101413-10-9
• Molecular Formula: 2C₄H₄O₄*C₂₅H₃₄N₄S
• Molecular Weight: 654.784

Synonyms:

Chemical Property of 2-{2-[4-(4-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine; compound with (E)-but-2-enedioic acid

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 2-{2-[4-(4-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine; compound with (E)-but-2-enedioic acid

There total 3 articles about 2-{2-[4-(4-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine; compound with (E)-but-2-enedioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4-(methylthio)phenyl)piperazine hydrochloride → 2-{2-[4-(4-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine; compound with (E)-but-2-enedioic acid (101413-10-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 38 percent / Et₃N / ethanol / 2 h / Heating

2: acetone

With triethylamine; In ethanol; acetone;

DOI:10.1248/cpb.33.5332

Reference yield:

2-(2-chloroethyl)-1,2,3,4,6,7,8,9-octahydrobenzo<1,6>naphthyridine dihydrochloride (83081-61-2) → 2-{2-[4-(4-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine; compound with (E)-but-2-enedioic acid (101413-10-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 38 percent / Et₃N / ethanol / 2 h / Heating

2: acetone

With triethylamine; In ethanol; acetone;

DOI:10.1248/cpb.33.5332

Reference yield:

2-{2-[4-(4-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine (101413-06-3) + (2E)-but-2-enedioic acid (110-17-8,26099-09-2) → 2-{2-[4-(4-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine; compound with (E)-but-2-enedioic acid (101413-10-9)

Guidance literature:

In acetone;

DOI:10.1248/cpb.33.5332

upstream raw materials:

2-{2-[4-(4-Methylsulfanyl-phenyl)-piperazin-1-yl]-ethyl}-1,2,3,4,6,7,8,9-octahydro-benzo[b][1,6]naphthyridine

(2E)-but-2-enedioic acid

2-(2-chloroethyl)-1,2,3,4,6,7,8,9-octahydrobenzo<1,6>naphthyridine dihydrochloride

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