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(1S,2R,5R,2'S)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-4-octenoate

Base Information Edit
  • Chemical Name:(1S,2R,5R,2'S)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-4-octenoate
  • CAS No.:100020-76-6
  • Molecular Formula:C24H36O3
  • Molecular Weight:372.548
  • Hs Code.:
  • Mol file:100020-76-6.mol
(1S,2R,5R,2'S)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-4-octenoate

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Chemical Property of (1S,2R,5R,2'S)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-4-octenoate Edit
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Technology Process of (1S,2R,5R,2'S)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-4-octenoate

There total 7 articles about (1S,2R,5R,2'S)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl 2-hydroxy-4-octenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 3 steps
1: 91 percent / 4-(dimethylamino)pyridine, triethylamine / CH2Cl2 / 1.5 h / 0 °C
2: 1.) osmium tetraoxide, 2.) sodium periodate / 1.) water, dioxane, RT, 5 min, 2.) RT, 2 h
3: 1.) tin tetrachloride, 2.) triethylamine / 1.) dichloromethane, -78 deg C, 10 min, 2.) -78 deg C, 6 h
With dmap; sodium periodate; osmium(VIII) oxide; tin(IV) chloride; triethylamine; In dichloromethane;
DOI:10.1021/jo00354a032
Guidance literature:
Multi-step reaction with 4 steps
1: 95 percent / p-toluenesulfonic acid monohydrate / benzene / 11 h / Heating
2: 81 percent / AgNO3 / acetonitrile / 94 h / Ambient temperature
3: 92 percent / sodium acetate trihydrate / dimethylsulfoxide / 1.17 h / Ambient temperature
4: 92 percent / SnCl4 / CH2Cl2 / -78 °C
With sodium acetate; tin(IV) chloride; toluene-4-sulfonic acid; silver nitrate; In dichloromethane; dimethyl sulfoxide; acetonitrile; benzene;
DOI:10.1016/S0040-4020(01)90590-3
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