4-(IODO-PHENYL)-METHANE SULFONYL CHLORIDE

Base Information

• Chemical Name: 4-(IODO-PHENYL)-METHANE SULFONYL CHLORIDE
• CAS No.: 345915-64-2
• Molecular Formula: C7H6ClIO2S
• Molecular Weight: 316.547
• Hs Code.: 2904990090
• Mol file: 345915-64-2.mol

Synonyms:4-iodobenzylamine*HCl;p-iodobenzylamine hydrochloride;4-iodobenzylsulfonyl chloride;4-IODOBENZYLAMINE,HYDROCHLORIDE SALT;4-iodobenzylamine hydrochloric acid salt;4-Jod-benzylamin,Hydrochlorid;4-iodo-benzylamine,hydrochloride;(4-iodophenyl)methanamine hydrochloride;(4-iodophenyl)methylamine,chloride;p-Iodbenzylsulfonylchlorid;

Chemical Property of 4-(IODO-PHENYL)-METHANE SULFONYL CHLORIDE

Chemical Property:

• PSA: 42.52000
• LogP: 3.44060

Purity/Quality:

99% ^*data from raw suppliers

4-(Iodo-phenyl)-methane sulfonyl chloride >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(IODO-PHENYL)-METHANE SULFONYL CHLORIDE

There total 2 articles about 4-(IODO-PHENYL)-METHANE SULFONYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

sodium (4-iodophenyl)methanesulfonate → (4-iodophenyl)methanesulfonyl chloride (345915-64-2)

Guidance literature:

With trichlorophosphate; In sulfolane; acetonitrile; at 60 ℃; for 2.5h;

DOI:10.1021/ol0158664

Reference yield:

→ (4-iodophenyl)methanesulfonyl chloride (345915-64-2)

Guidance literature:

Na-Salz von p-Iodbenzylsulfonsaeure, PCl5;

DOI:10.1007/BF01199621

Reference yield: 93.0%

2,2-dimethyl-propanol-1 (75-84-3) + (4-iodophenyl)methanesulfonyl chloride (345915-64-2) → neopentyl (4-iodo-phenyl)methanesulfonate

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 20h;

DOI:10.1021/ol0158664

Downstream raw materials:

2,2,2-trichloroethyl (4-iodo-phenyl)methanesulfonate

N,N-bis(2,4-dimethoxybenzyl)-1-(4-iodophenyl)methanesulfonamide

N,N-bis(2,4-dimethoxybenzyl)-1,1-difluoro-1-(4-iodophenyl)methanesulfonamide

(S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(4-(difluoro((neopentyloxy)sulfonyl)methyl)phenyl)propanoic acid

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