(3-(Chloromethyl)oxetan-3-yl)methanol

Base Information

• Chemical Name: (3-(Chloromethyl)oxetan-3-yl)methanol
• CAS No.: 4351-77-3
• Molecular Formula: C5H9ClO2
• Molecular Weight: 136.58
• Hs Code.: 2932999099
• Mol file: 4351-77-3.mol

Synonyms:(3-chloromethyl-oxetan-3-yl)-methanol;3-chloromethyl-3-hydroxymethyl-oxetane;3-chloromethyl-2-methyl-pyridine 1-oxide;3-Chlormethyl-3-hydroxymethyl-oxetan;3-chloromethyl-2-methylpyridine-N-oxide;3-(hydroxymethyl)-3-chloromethyl oxetane;Pyridine,3-(chloromethyl)-2-methyl-,1-oxide;

Chemical Property of (3-(Chloromethyl)oxetan-3-yl)methanol

Chemical Property:

• Boiling Point: 221.4 °C at 760 mmHg
• Flash Point: 87.7 °C
• PSA: 29.46000
• Density: 1.225 g/cm³
• LogP: 0.23410

Purity/Quality:

97% ^*data from raw suppliers

(3-(Chloromethyl)oxetan-3-yl)methanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-(Chloromethyl)oxetan-3-yl)methanol

There total 3 articles about (3-(Chloromethyl)oxetan-3-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-bis(chloromethyl)-1,3-propanediol (2209-86-1) → 3-(hydroxymethyl)-3-chloromethyl oxetane (4351-77-3)

Guidance literature:

With potassium hydroxide;

DOI:10.1039/jr9550003648

Reference yield:

Pentaerythritol (115-77-5) → 3-(hydroxymethyl)-3-chloromethyl oxetane (4351-77-3)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂, pyridine / 14 h / Heating

2: KOH / ethanol / 5 h / Heating

With pyridine; potassium hydroxide; thionyl chloride; In ethanol;

DOI:10.1016/S0022-1139(00)80471-6

Reference yield:

→ 3-(hydroxymethyl)-3-chloromethyl oxetane (4351-77-3)

Guidance literature:

aus 3,3-Bis(chlormethyl)oxetan I;

upstream raw materials:

2,2-bis(chloromethyl)-1,3-propanediol

Pentaerythritol

Downstream raw materials:

2,6-dioxaspiro<3.3>heptane

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