Technology Process of C24H22Cl2N2O2
There total 3 articles about C24H22Cl2N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide; nickel-aluminum alloy / ethanol; water
2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 20 °C
3.1: boron tribromide / dichloromethane
4.1: triethylamine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
4.2: 20 °C / Inert atmosphere
With
nickel-aluminum alloy; boron tribromide; potassium carbonate; triethylamine; potassium iodide; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.09.005
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 20 °C
2.1: boron tribromide / dichloromethane
3.1: triethylamine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
With
boron tribromide; potassium carbonate; triethylamine; potassium iodide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.09.005
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: boron tribromide / dichloromethane
2.1: triethylamine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
With
boron tribromide; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmc.2012.09.005
