1-phenyl-2-methyl-4-benzoyl-5-iodobenzimidazole

Base Information

Chemical Name:1-phenyl-2-methyl-4-benzoyl-5-iodobenzimidazole
CAS No.:107451-03-6
Molecular Formula:C₂₁H₁₅IN₂O
Molecular Weight:438.267
Hs Code.:

Synonyms:

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Chemical Property of 1-phenyl-2-methyl-4-benzoyl-5-iodobenzimidazole

Chemical Property:

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Technology Process of 1-phenyl-2-methyl-4-benzoyl-5-iodobenzimidazole

There total 4 articles about 1-phenyl-2-methyl-4-benzoyl-5-iodobenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14625-61-7
2-methyl-5-nitro-1-phenyl-1H-benzo[d]imidazole

: 107451-03-6
1-phenyl-2-methyl-4-benzoyl-5-iodobenzimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaOH / methanol / 5 h / Heating

2: 89 percent / N₂H_4.H₂O / Raney Ni / ethanol / 4 h / Heating

3: 1.conc.HCl, NaNO₂ 2.KI / 1.CH₃COOH,H₂O,6 grad C,150min 2. 5 grad C,3h,towards the end 35 grad C

With hydrogenchloride; sodium hydroxide; hydrazine hydrate; potassium iodide; sodium nitrite; nickel; In methanol; ethanol;
DOI:10.1007/BF01175063

Reference yield:

: 140-29-4
phenylacetonitrile

: 107451-03-6
1-phenyl-2-methyl-4-benzoyl-5-iodobenzimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaOH / methanol / 5 h / Heating

2: 89 percent / N₂H_4.H₂O / Raney Ni / ethanol / 4 h / Heating

3: 1.conc.HCl, NaNO₂ 2.KI / 1.CH₃COOH,H₂O,6 grad C,150min 2. 5 grad C,3h,towards the end 35 grad C

With hydrogenchloride; sodium hydroxide; hydrazine hydrate; potassium iodide; sodium nitrite; nickel; In methanol; ethanol;
DOI:10.1007/BF01175063

Reference yield:

: 89174-96-9
3,6-diphenyl-5-methylimidazo<4,5-e>-2,1-benzisoxazole

: 107451-03-6
1-phenyl-2-methyl-4-benzoyl-5-iodobenzimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / N₂H_4.H₂O / Raney Ni / ethanol / 4 h / Heating

2: 1.conc.HCl, NaNO₂ 2.KI / 1.CH₃COOH,H₂O,6 grad C,150min 2. 5 grad C,3h,towards the end 35 grad C

With hydrogenchloride; hydrazine hydrate; potassium iodide; sodium nitrite; nickel; In ethanol;
DOI:10.1007/BF01175063