Technology Process of C42H32Cl2N4O
There total 6 articles about C42H32Cl2N4O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1021/ja1102844
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 20 - 80 °C
2.1: sodium azide; trifluoroacetic acid / 0 °C
2.2: 0.5 h / 0 °C
3.1: ammonium formate; zinc / methanol / 15 h / 20 °C / Inert atmosphere
4.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere
With
pyridine; sodium azide; copper(ll) sulfate pentahydrate; ammonium formate; sodium L-ascorbate; trifluoroacetic acid; zinc;
In
methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ja1102844
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium azide; trifluoroacetic acid / 0 °C
1.2: 0.5 h / 0 °C
2.1: ammonium formate; zinc / methanol / 15 h / 20 °C / Inert atmosphere
3.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere
With
pyridine; sodium azide; ammonium formate; trifluoroacetic acid; zinc;
In
methanol; dichloromethane;
DOI:10.1021/ja1102844