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Technology Process of trans-{Rh(1,3:4,6-bis(1,4-(9-(1-benzimidazolyl)-1,4,7-trioxanonyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl2}Cl*7H2O

trans-{Rh(1,3:4,6-bis(1,4-(9-(1-benzimidazolyl)-1,4,7-trioxanonyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl2}Cl*7H2O

Base Information
  • Chemical Name:trans-{Rh(1,3:4,6-bis(1,4-(9-(1-benzimidazolyl)-1,4,7-trioxanonyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl2}Cl*7H2O
  • CAS No.:118715-79-0
  • Molecular Formula:C84H90Cl2N12O14Rh*Cl*7H2O
  • Molecular Weight:1827.08
  • Hs Code.:
trans-{Rh(1,3:4,6-bis(1,4-(9-(1-benzimidazolyl)-1,4,7-trioxanonyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl<sub>2</sub>}Cl*7H<sub>2</sub>O

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Chemical Property of trans-{Rh(1,3:4,6-bis(1,4-(9-(1-benzimidazolyl)-1,4,7-trioxanonyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl2}Cl*7H2O
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Technology Process of trans-{Rh(1,3:4,6-bis(1,4-(9-(1-benzimidazolyl)-1,4,7-trioxanonyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl2}Cl*7H2O

There total 1 articles about trans-{Rh(1,3:4,6-bis(1,4-(9-(1-benzimidazolyl)-1,4,7-trioxanonyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl2}Cl*7H2O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

rhodium(III) chloride trihydrate

rhodium(III) chloride trihydrate

1,3:4,6-bis(1,4-(9-(1-benzimidazolyl)-1,4,7-trioxanonyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H,4H,6H)-dione
118715-70-1

1,3:4,6-bis(1,4-(9-(1-benzimidazolyl)-1,4,7-trioxanonyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H,4H,6H)-dione

trans-{Rh(1,3:4,6-bis(1,4-(9-(1-benzimidazolyl)-1,4,7-trioxanonyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl<sub>2</sub>}Cl*7H<sub>2</sub>O
118715-79-0

trans-{Rh(1,3:4,6-bis(1,4-(9-(1-benzimidazolyl)-1,4,7-trioxanonyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H)-dione)Cl2}Cl*7H2O

Guidance literature:
In methanol; 16 h at reflux temperature; filtration, evapd. in vac., elem. anal;
DOI:10.1021/ja00188a022
upstream raw materials:

1,3:4,6-bis(1,4-(9-(1-benzimidazolyl)-1,4,7-trioxanonyl)-2,3-xylylene)-tetrahydro-3a,6a-diphenylimidazo{4,5-d}imidazole-2,5(1H,3H,4H,6H)-dione

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