C₃₄H₅₀O₅Si

Base Information

Chemical Name:C₃₄H₅₀O₅Si
CAS No.:1391853-34-1
Molecular Formula:C₃₄H₅₀O₅Si
Molecular Weight:566.853
Hs Code.:

C<sub>34</sub>H<sub>50</sub>O<sub>5</sub>Si

Synonyms:

Suppliers and Price of C₃₄H₅₀O₅Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₄H₅₀O₅Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₄H₅₀O₅Si

There total 11 articles about C₃₄H₅₀O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(3-(1,4-dioxaspiro[4.5]decan-2-yl)propylsulfonyl)benzo[d]thiazole

: 1245726-24-2
(5S,6S)-6-(tert-butyldiphenylsilyloxymethyl)-5-methyltetrahydro-2H-pyran-2-one

: 1391853-34-1
C₃₄H₅₀O₅Si

Guidance literature:: 2-(3-(1,4-dioxaspiro[4.5]decan-2-yl)propylsulfonyl)benzo[d]thiazole; (5S,6S)-6-(tert-butyldiphenylsilyloxymethyl)-5-methyltetrahydro-2H-pyran-2-one; With boron trifluoride diethyl etherate; lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

With acetic acid; In tetrahydrofuran; at -78 - 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1002/chem.201102462

Reference yield:

: 885051-17-2
ethyl (2E,4S)-5-(tert-butyldiphenylsilanyloxy)-4-hydroxy-2-pentenoate

: 1391853-34-1
C₃₄H₅₀O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridinium p-toluenesulfonate / dichloromethane / 16 h / Inert atmosphere; Reflux

2.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 0.25 h / -20 - -10 °C / Inert atmosphere

2.2: 5 h / -78 - -50 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

5.1: pyridinium p-toluenesulfonate / 1,4-dioxane; water / 4 h / 70 °C

6.1: pyridinium chlorochromate / dichloromethane / 5 h / 20 °C / Inert atmosphere; Molecular sieve

7.1: boron trifluoride diethyl etherate; lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

7.2: 0.25 h / -78 - 20 °C / Inert atmosphere

With copper(l) iodide; boron trifluoride diethyl etherate; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; pyridinium chlorochromate; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water;
DOI:10.1002/chem.201102462

Reference yield:

: ethyl (4S,E)-5-(tert-butyldiphenylsilyloxy)-4-(tetrahydro-2H-pyran-2-yloxy)pent-2-enoate

: 1391853-34-1
C₃₄H₅₀O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 0.25 h / -20 - -10 °C / Inert atmosphere

1.2: 5 h / -78 - -50 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: pyridinium p-toluenesulfonate / 1,4-dioxane; water / 4 h / 70 °C

5.1: pyridinium chlorochromate / dichloromethane / 5 h / 20 °C / Inert atmosphere; Molecular sieve

6.1: boron trifluoride diethyl etherate; lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

6.2: 0.25 h / -78 - 20 °C / Inert atmosphere

With copper(l) iodide; boron trifluoride diethyl etherate; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; pyridinium chlorochromate; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water;
DOI:10.1002/chem.201102462