C₃₇H₄₈O₅Si

Base Information

Chemical Name:C₃₇H₄₈O₅Si
CAS No.:1323858-62-3
Molecular Formula:C₃₇H₄₈O₅Si
Molecular Weight:600.871
Hs Code.:

C<sub>37</sub>H<sub>48</sub>O<sub>5</sub>Si

Synonyms:

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Chemical Property of C₃₇H₄₈O₅Si

Chemical Property:

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Technology Process of C₃₇H₄₈O₅Si

There total 16 articles about C₃₇H₄₈O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1323858-23-6
C₃₇H₄₈O₆Si

: 1323858-20-3
C₃₇H₄₆O₅Si

: 1323858-62-3
C₃₇H₄₈O₅Si

Guidance literature:: With ferrous(II) sulfate heptahydrate; copper diacetate; In methanol; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201101893

Reference yield:

: 934985-87-2
C₂₃H₃₇BrO₃

: 1323858-20-3
C₃₇H₄₆O₅Si

: 1323858-62-3
C₃₇H₄₈O₅Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: 1H-imidazole / dichloromethane / 0.5 h / 20 °C

2.1: iodine; lead(IV) tetraacetate; calcium carbonate / cyclohexane / 2 h / Reflux; Irradiation

3.1: Jones reagent / acetone / 0 °C

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 24 h / 120 °C

5.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile); cyclohexane-1,2-epoxide / tetrachloromethane / 1 h / Reflux

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.33 h / 0 - 50 °C

7.1: ozone / dichloromethane / 0.6 h / -78 °C

7.2: 24 h / 20 °C / Inert atmosphere

8.1: [bis(acetoxy)iodo]benzene; iodine / cyclohexane / 1 h / Irradiation

9.1: pyridinium p-toluenesulfonate / 20 - 130 °C

10.1: methanol; triethylamine / 14 h / 50 °C

11.1: triethylamine / dichloromethane / 3 h / 0 °C

12.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

13.1: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 0.5 h / 0 °C / Irradiation

14.1: ferrous(II) sulfate heptahydrate; copper diacetate / methanol / 1 h / 20 °C / Inert atmosphere

With 1H-imidazole; methanol; ferrous(II) sulfate heptahydrate; lithium aluminium tetrahydride; Jones reagent; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile); [bis(acetoxy)iodo]benzene; iodine; oxygen; copper diacetate; lead(IV) tetraacetate; pyridinium p-toluenesulfonate; 5,15,10,20-tetraphenylporphyrin; cyclohexane-1,2-epoxide; ozone; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; calcium carbonate; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; cyclohexane; acetone; toluene; 13.1: Schenck ene reaction;
DOI:10.1002/anie.201101893

Reference yield:

: C₃₇H₅₁BrO₃Si

: 1323858-20-3
C₃₇H₄₆O₅Si

: 1323858-62-3
C₃₇H₄₈O₅Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: Jones reagent / acetone / 0 °C

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 24 h / 120 °C

3.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile); cyclohexane-1,2-epoxide / tetrachloromethane / 1 h / Reflux

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.33 h / 0 - 50 °C

5.1: ozone / dichloromethane / 0.6 h / -78 °C

5.2: 24 h / 20 °C / Inert atmosphere

6.1: [bis(acetoxy)iodo]benzene; iodine / cyclohexane / 1 h / Irradiation

7.1: pyridinium p-toluenesulfonate / 20 - 130 °C

8.1: methanol; triethylamine / 14 h / 50 °C

9.1: triethylamine / dichloromethane / 3 h / 0 °C

10.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

11.1: oxygen; 5,15,10,20-tetraphenylporphyrin / dichloromethane / 0.5 h / 0 °C / Irradiation

12.1: ferrous(II) sulfate heptahydrate; copper diacetate / methanol / 1 h / 20 °C / Inert atmosphere

With methanol; ferrous(II) sulfate heptahydrate; lithium aluminium tetrahydride; Jones reagent; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile); [bis(acetoxy)iodo]benzene; iodine; oxygen; copper diacetate; pyridinium p-toluenesulfonate; 5,15,10,20-tetraphenylporphyrin; cyclohexane-1,2-epoxide; ozone; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; cyclohexane; acetone; toluene; 11.1: Schenck ene reaction;
DOI:10.1002/anie.201101893