1-{(3aR,4R,6R,6aR)-6-[(R)-1-Azido-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-1H-pyrimidine-2,4-dione

Base Information

Chemical Name:1-{(3aR,4R,6R,6aR)-6-[(R)-1-Azido-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-1H-pyrimidine-2,4-dione
CAS No.:174498-69-2
Molecular Formula:C₂₉H₃₅N₅O₆Si
Molecular Weight:577.712
Hs Code.:

1-{(3aR,4R,6R,6aR)-6-[(R)-1-Azido-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-1H-pyrimidine-2,4-dione

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Chemical Property of 1-{(3aR,4R,6R,6aR)-6-[(R)-1-Azido-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-1H-pyrimidine-2,4-dione

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Technology Process of 1-{(3aR,4R,6R,6aR)-6-[(R)-1-Azido-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-1H-pyrimidine-2,4-dione

There total 1 articles about 1-{(3aR,4R,6R,6aR)-6-[(R)-1-Azido-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₃₄N₂O₆Si

: 174498-69-2
1-{(3aR,4R,6R,6aR)-6-[(R)-1-Azido-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-1H-pyrimidine-2,4-dione

Guidance literature:: With sodium azide; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 80 ℃;
DOI:10.1016/0040-4039(95)02116-7

Reference yield:

: 174498-69-2
1-{(3aR,4R,6R,6aR)-6-[(R)-1-Azido-2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-1H-pyrimidine-2,4-dione

: 24695-48-5
1-(5'-amino-5'-deoxy-α-D-allofuranuronosyl)uracil

Guidance literature:: Multi-step reaction with 4 steps

1: TBAF / tetrahydrofuran

2: PDC / dimethylformamide

3: formic acid / H₂O

4: H₂ / Pd/C / methanol; H₂O

With dipyridinium dichromate; formic acid; tetrabutyl ammonium fluoride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(95)02116-7