Nitroacetonitrile

Base Information

• Chemical Name: Nitroacetonitrile
• CAS No.: 13218-13-8
• Molecular Formula: C2H2N2O2
• Molecular Weight: 86.0501
• Hs Code.: 2926909090
• Mol file: 13218-13-8.mol

Synonyms:NITROACETONITRILE;

Chemical Property of Nitroacetonitrile

Chemical Property:

• Boiling Point: 224.4 °C at 760 mmHg
• PKA: 4.62±0.29(Predicted)
• Flash Point: 89.5 °C
• PSA: 69.61000
• Density: 1.27 g/cm³
• LogP: 0.30988

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Nitroacetonitrile

There total 8 articles about Nitroacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1,2-dinitroethane (7570-26-5) → nitroacetonitrile (13218-13-8)

Guidance literature:

With thionyl chloride; In diethyl ether; for 1h; Heating;

DOI:10.1002/jhet.5570320349

Reference yield: 85.0%

(E)-3-Hydroxy-2-nitro-but-2-enenitrile → nitroacetonitrile (13218-13-8)

Guidance literature:

With sulfuric acid; In methanol; for 1h;

DOI:10.1007/BF00699138

Reference yield: 58.0%

2-nitroacetaldehyde oxime (5653-21-4) → nitroacetonitrile (13218-13-8)

Guidance literature:

With thionyl chloride; In diethyl ether; for 1h; Heating;

DOI:10.1021/jm00156a024

upstream raw materials:

metazonic acid

2-Nitro-3-oxo-propionitrile

2-nitroacetaldehyde oxime

1,2-dinitroethane

Downstream raw materials:

2-nitroacetamide

2,2'-dinitro-2,2'-cyclohexylidene-di-acetonitrile; bis-diethylamine salt

(E)-1-cyano-2-(4'-chlorophenyl)-1-nitroethene

3-anilino-2-nitro-3-phenyl-propionitrile