C₃₃H₅₂O₈

Base Information

Chemical Name:C₃₃H₅₂O₈
CAS No.:1429481-15-1
Molecular Formula:C₃₃H₅₂O₈
Molecular Weight:576.771
Hs Code.:

C<sub>33</sub>H<sub>52</sub>O<sub>8</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₅₂O₈

Chemical Property:

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Technology Process of C₃₃H₅₂O₈

There total 6 articles about C₃₃H₅₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₅₂O₇

: 1429481-15-1
C₃₃H₅₂O₈

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -40 - 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo400263w

Reference yield:

: 1429481-14-0
tert-butyl (4aS,6R,7R,7aS)-7-(benzyloxy)-4a-dodecyltetrahydro-6-(hydroxymethyl)-2,2-dimethyl-4H-furo[3,2-d][1,3]-dioxine-7a-carboxylate

: 1429481-15-1
C₃₃H₅₂O₈

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Cooling with ice; Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid; sodium hydrogencarbonate / dichloromethane / 2 h / -40 - 0 °C / Inert atmosphere

With sodium hydrogencarbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo400263w

Reference yield:

: C₂₂H₂₂O₈

: 1429481-15-1
C₃₃H₅₂O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

2.1: water; toluene-4-sulfonic acid / 16 h / Inert atmosphere; Reflux

3.1: diisobutylaluminium hydride / hexane; toluene / 1 h / -78 °C / Inert atmosphere

4.1: n-butyllithium / hexane; dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere

4.2: 4 h / 120 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Cooling with ice; Inert atmosphere

6.1: 3-chloro-benzenecarboperoxoic acid; sodium hydrogencarbonate / dichloromethane / 2 h / -40 - 0 °C / Inert atmosphere

With n-butyllithium; oxalyl dichloride; water; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; In hexane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo400263w