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Technology Process of Sitagliptin EP Impurity B

Sitagliptin EP Impurity B

Base Information
  • Chemical Name:Sitagliptin EP Impurity B
  • CAS No.:1345822-87-8
  • Molecular Formula:C16H16F5N5O*H3O4P
  • Molecular Weight:487.323
  • Hs Code.:
  • Mol file:1345822-87-8.mol
Sitagliptin EP Impurity B

Synonyms:

Suppliers and Price of Sitagliptin EP Impurity B
Supply Marketing:
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • TRC
  • 4-DesfluoroSitagliptin
  • 25mg
  • $ 1320.00
Total 6 raw suppliers
Chemical Property of Sitagliptin EP Impurity B
Chemical Property:
Purity/Quality:

99%, *data from raw suppliers

4-DesfluoroSitagliptin *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
  • Uses 4-Desfluoro Sitagliptin is a metabolite of Sitagliptin phosphate (S491000). Sitagliptin is a trizolopyrazine dipeptidyl peptidase IV inhibitor. Sitagliptin has recently been approved for the therapy of type II diabetes.
Technology Process of Sitagliptin EP Impurity B

There total 1 articles about Sitagliptin EP Impurity B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3R)-3-amino-1-[3-(trifluoromethyl)-5H,6H,7H,8H [1,2,4] triazolo [4,3-a]pyrazin-7-yl]-4-(2,5-difluorophenyl) butan-1-one phosphate
1345822-87-8

(3R)-3-amino-1-[3-(trifluoromethyl)-5H,6H,7H,8H [1,2,4] triazolo [4,3-a]pyrazin-7-yl]-4-(2,5-difluorophenyl) butan-1-one phosphate

Guidance literature:
With palladium 10% on activated carbon; hydrogen; benzyl chloride; In ethanol; water; at 40 ℃; under 2068.65 Torr; Autoclave; Inert atmosphere;
With phosphoric acid; In ethanol; water; at 75 ℃;
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