C₂₈H₃₂ClNO₃

Base Information

Chemical Name:C₂₈H₃₂ClNO₃
CAS No.:1256254-58-6
Molecular Formula:C₂₈H₃₂ClNO₃
Molecular Weight:466.02
Hs Code.:

C<sub>28</sub>H<sub>32</sub>ClNO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₃₂ClNO₃

Chemical Property:

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Technology Process of C₂₈H₃₂ClNO₃

There total 4 articles about C₂₈H₃₂ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4664-13-5
2,4-dihydroxy-3,6-dimethylpyridine

: 1256254-58-6
C₂₈H₃₂ClNO₃

Guidance literature:: Multi-step reaction with 7 steps

1: bromine / dichloromethane

2: Dichlorophenylphosphine; chlorine / Heating

3: isopropylmagnesium chloride lithium chloride complex / tetrahydrofuran / -20 °C

4: benzo[1,3,2]dioxaborole / benzene

5: perchloric acid

6: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / water; N,N-dimethyl-formamide

7: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium carbonate / water; N,N-dimethyl acetamide

With bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; perchloric acid; isopropylmagnesium chloride lithium chloride complex; bromine; chlorine; sodium carbonate; Dichlorophenylphosphine; benzo[1,3,2]dioxaborole; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; benzene; 6: |Suzuki Coupling;
DOI:10.1021/ml500110j

Reference yield:

: 1256254-38-2
C₁₀H₉Cl₂NO₃

: 1256254-58-6
C₂₈H₃₂ClNO₃

Guidance literature:: Multi-step reaction with 4 steps

1: benzo[1,3,2]dioxaborole / benzene

2: perchloric acid

3: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / water; N,N-dimethyl-formamide

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium carbonate / water; N,N-dimethyl acetamide

With bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; perchloric acid; sodium carbonate; benzo[1,3,2]dioxaborole; In N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; benzene; 3: |Suzuki Coupling;
DOI:10.1021/ml500110j

Reference yield:

: 1256254-43-9
C₁₄H₁₉Cl₂NO₃

: 1256254-58-6
C₂₈H₃₂ClNO₃

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / water; N,N-dimethyl-formamide

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium carbonate / water; N,N-dimethyl acetamide

With bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium carbonate; In N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; 1: |Suzuki Coupling;
DOI:10.1021/ml500110j