C₂HF₃O₂*C₉H₁₀Br₃NO

Base Information

Chemical Name:C₂HF₃O₂*C₉H₁₀Br₃NO
CAS No.:1359741-01-7
Molecular Formula:C₂HF₃O₂*C₉H₁₀Br₃NO
Molecular Weight:501.92
Hs Code.:

C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>9</sub>H<sub>10</sub>Br<sub>3</sub>NO

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Chemical Property of C₂HF₃O₂*C₉H₁₀Br₃NO

Chemical Property:

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Technology Process of C₂HF₃O₂*C₉H₁₀Br₃NO

There total 7 articles about C₂HF₃O₂*C₉H₁₀Br₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1359715-00-6
2-(2,3,4-tribromo-5-methoxyphenyl)ethanamine hydrochloride

: 1359741-01-7
C₂HF₃O₂*C₉H₁₀Br₃NO

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; water / 0 - 20 °C

2: dichloromethane / 0.42 h / 0 °C

With sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo3000173

Reference yield:

: 1359714-96-7
2,3,4-tribromo-5-methoxybenzaldehyde

: 1359741-01-7
C₂HF₃O₂*C₉H₁₀Br₃NO

Guidance literature:: Multi-step reaction with 6 steps

1: ammonium acetate / 5 h / Reflux

2: borane-dimethyl sulfide complex / tetrahydrofuran / 0.33 h / 0 °C

3: sodium tetrahydroborate / tetrahydrofuran / 156 h / 20 °C

4: hydrogenchloride / 1,4-dioxane; chloroform

5: sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; water / 0 - 20 °C

6: dichloromethane / 0.42 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; borane-dimethyl sulfide complex; ammonium acetate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; chloroform; water;
DOI:10.1021/jo3000173

Reference yield:

: 1359715-20-0
C₈H₇Br₃O₂

: 1359741-01-7
C₂HF₃O₂*C₉H₁₀Br₃NO

Guidance literature:: Multi-step reaction with 7 steps

1: pyridinium chlorochromate / dichloromethane / 60 h / 0 - 20 °C

2: ammonium acetate / 5 h / Reflux

3: borane-dimethyl sulfide complex / tetrahydrofuran / 0.33 h / 0 °C

4: sodium tetrahydroborate / tetrahydrofuran / 156 h / 20 °C

5: hydrogenchloride / 1,4-dioxane; chloroform

6: sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; water / 0 - 20 °C

7: dichloromethane / 0.42 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; borane-dimethyl sulfide complex; ammonium acetate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; chloroform; water;
DOI:10.1021/jo3000173