1--3-hydroxy-6-methylpyridinium chloride

Base Information

Chemical Name:1--3-hydroxy-6-methylpyridinium chloride
CAS No.:74780-47-5
Molecular Formula:C₁₅H₁₃BrNO₂*Cl
Molecular Weight:354.631
Hs Code.:

1-<trans-3-(4-bromophenyl)-3-oxoprop-1-enyl>-3-hydroxy-6-methylpyridinium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1--3-hydroxy-6-methylpyridinium chloride

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Technology Process of 1--3-hydroxy-6-methylpyridinium chloride

There total 1 articles about 1--3-hydroxy-6-methylpyridinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1121-78-4
5-Hydroxy-2-methylpyridine

: 58953-16-5
(E)-3-chloro-1-(4-bromophenyl)-2-propenone

: 74780-47-5
1--3-hydroxy-6-methylpyridinium chloride

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1039/P19800000362

Reference yield:

: 74780-47-5
1--3-hydroxy-6-methylpyridinium chloride

: 74780-70-4
3,7,8-trimethyl-2--3-endo-2-azabicyclo<4.3.1>deca-3,7-dien-10-one

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / triethylamine / acetonitrile

2: 25 percent / hydroquinone / acetonitrile / 8 h / 70 °C

With triethylamine; hydroquinone; In acetonitrile;
DOI:10.1039/P19800000362