Technology Process of C4H6O4*C22H24Cl3N3O2
There total 6 articles about C4H6O4*C22H24Cl3N3O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium hydroxide / N,N-dimethyl-formamide / 100 °C
2: hydrogenchloride; water / ethanol / Reflux
3: phosphoric acid / 100 °C
4: palladium on activated charcoal; hydrazine hydrate / ethanol / Reflux
5: sodium tetrahydroborate; acetic acid / 20 °C
6: hydrazine hydrate / ethanol / Reflux
7: ethanol
With
hydrogenchloride; sodium tetrahydroborate; phosphoric acid; palladium on activated charcoal; water; hydrazine hydrate; acetic acid; potassium hydroxide;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.12.108
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrazine hydrate / ethanol / Reflux
2: ethanol
With
hydrazine hydrate;
In
ethanol;
DOI:10.1016/j.bmcl.2011.12.108
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrogenchloride; water / ethanol / Reflux
2: phosphoric acid / 100 °C
3: palladium on activated charcoal; hydrazine hydrate / ethanol / Reflux
4: sodium tetrahydroborate; acetic acid / 20 °C
5: hydrazine hydrate / ethanol / Reflux
6: ethanol
With
hydrogenchloride; sodium tetrahydroborate; phosphoric acid; palladium on activated charcoal; water; hydrazine hydrate; acetic acid;
In
ethanol;
DOI:10.1016/j.bmcl.2011.12.108