Technology Process of C55H76N2O13Si
There total 8 articles about C55H76N2O13Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 75 percent / p-TsOH / methanol
2: 92 percent / Py
3: 72 percent / silica gel / acetonitrile; tetrahydrofuran / 55 °C
4: 100 percent / HF*Py
5: 89 percent / LiHMDS / tetrahydrofuran
6: OsO4; N-methylmorpholine N-oxide
7: NaIO4
8: AcOH; NaBH3CN
With
pyridine; sodium periodate; osmium(VIII) oxide; silica gel; sodium cyanoborohydride; toluene-4-sulfonic acid; pyridine hydrogenfluoride; acetic acid; 4-methylmorpholine N-oxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; acetonitrile;
DOI:10.1016/S0960-894X(00)00682-X
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 89 percent / LiHMDS / tetrahydrofuran
2: OsO4; N-methylmorpholine N-oxide
3: NaIO4
4: AcOH; NaBH3CN
With
sodium periodate; osmium(VIII) oxide; sodium cyanoborohydride; acetic acid; 4-methylmorpholine N-oxide; lithium hexamethyldisilazane;
In
tetrahydrofuran;
DOI:10.1016/S0960-894X(00)00682-X
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 100 percent / HF*Py
2: 89 percent / LiHMDS / tetrahydrofuran
3: OsO4; N-methylmorpholine N-oxide
4: NaIO4
5: AcOH; NaBH3CN
With
sodium periodate; osmium(VIII) oxide; sodium cyanoborohydride; pyridine hydrogenfluoride; acetic acid; 4-methylmorpholine N-oxide; lithium hexamethyldisilazane;
In
tetrahydrofuran;
DOI:10.1016/S0960-894X(00)00682-X