p-chloro-phenyl-3 endo bicyclo<2.2.1> heptene-5 carboxylate endo-2 de methyle

Base Information

Chemical Name:p-chloro-phenyl-3 endo bicyclo<2.2.1> heptene-5 carboxylate endo-2 de methyle
CAS No.:81509-26-4
Molecular Formula:C₁₅H₁₅ClO₂
Molecular Weight:262.736
Hs Code.:

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Chemical Property of p-chloro-phenyl-3 endo bicyclo<2.2.1> heptene-5 carboxylate endo-2 de methyle

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Technology Process of p-chloro-phenyl-3 endo bicyclo<2.2.1> heptene-5 carboxylate endo-2 de methyle

There total 8 articles about p-chloro-phenyl-3 endo bicyclo<2.2.1> heptene-5 carboxylate endo-2 de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 59259-40-4,59286-06-5,59286-10-1,81570-33-4
(+/-)-3endo-(4-chloro-phenyl)-norborn-5-ene-2exo-carboxylic acid

: 81509-26-4,81570-39-0,81570-44-7
p-chloro-phenyl-3 endo bicyclo<2.2.1>heptene-5 carboxylate exo-2 de methyle

Guidance literature:: methylation;
DOI:10.1016/S0040-4020(01)98883-0

Reference yield: 70.0%

: 59259-40-4,59286-06-5,59286-10-1,81570-33-4
(+/-)-3exo-(4-chloro-phenyl)-norborn-5-ene-2endo-carboxylic acid

: 81509-26-4,81570-39-0,81570-44-7
p-chloro-phenyl-3 exo bicyclo<2.2.1> heptene-5 carboxylate endo-2 de methyle

Guidance literature:: methylation;
DOI:10.1016/S0040-4020(01)98883-0

Reference yield:

: 1615-02-7,940-62-5
3-(4-chlorophenyl)prop-2-enoic acid

: 81509-26-4,81570-39-0,81570-44-7
p-chloro-phenyl-3 endo bicyclo<2.2.1> heptene-5 carboxylate endo-2 de methyle

Guidance literature:: Multi-step reaction with 4 steps

1: 43 percent / dioxane / 45 h / Irradiation

2: 2.) I₂ / 1.) toluene, reflux, 7 d.

3: 65 percent

4: 88 percent / methylation

With iodine; In 1,4-dioxane;
DOI:10.1016/S0040-4020(01)98883-0