C₄₆H₅₆O₁₀

Base Information

Chemical Name:C₄₆H₅₆O₁₀
CAS No.:725253-52-1
Molecular Formula:C₄₆H₅₆O₁₀
Molecular Weight:768.945
Hs Code.:

C<sub>46</sub>H<sub>56</sub>O<sub>10</sub>

Synonyms:

Suppliers and Price of C₄₆H₅₆O₁₀

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₆H₅₆O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₆H₅₆O₁₀

There total 16 articles about C₄₆H₅₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 725253-51-0
C₄₇H₅₈O₁₁

: 725253-52-1
C₄₆H₅₆O₁₀

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; acetonitrile; at -15 ℃;
DOI:10.1016/j.tetlet.2004.04.083

Reference yield:

: 252046-22-3
(2R,3R,4S,4aS,9aS)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-2,3,4,4a,9,9a-hexahydro-6H-pyrano[3,2-b]oxepin

: 725253-52-1
C₄₆H₅₆O₁₀

Guidance literature:: Multi-step reaction with 15 steps

1.1: AD-mix β; MeSO2NH2 / 2-methyl-propan-2-ol; H2O; various solvent(s) / 0 °C

2.1: CSA / CH₂Cl₂ / 20 °C

3.1: H₂ / Pd/C / ethyl acetate; methanol / 20 °C

4.1: CSA / CH₂Cl₂ / 20 °C

5.1: 92 percent / KOt-Bu; n-Bu₄NI / tetrahydrofuran / 20 °C

6.1: 100 percent / DIBAL-H / CH₂Cl₂ / -78 - 0 °C

7.1: 92 percent / I₂; PPh₃; imidazole / tetrahydrofuran / 20 °C

8.1: 99 percent / NaH / dimethylformamide / 0 - 20 °C

9.1: 9-BBN / tetrahydrofuran / 20 °C

9.2: aq. Cs₂CO₃ / PdCl₂(dppf)*CH₂Cl₂ / tetrahydrofuran; dimethylformamide / 50 °C

10.1: thexylborane / tetrahydrofuran / 0 °C

10.2: 78 percent / aq. NaOH; aq. H₂O₂ / tetrahydrofuran / 20 °C

11.1: TPAP; NMO; 4 Angstroem molecular sieves / CH₂Cl₂ / 20 °C

12.1: TMSCl; LiHMDS; Et₃N / tetrahydrofuran / -78 °C

12.2: Pd(OAc)2 / acetonitrile / 20 °C

13.1: 85 percent / DDQ / CH₂Cl₂ / 20 °C / pH 7

14.1: PPTS / toluene / 50 °C

15.1: Et₃SiH; BF₃*OEt₂ / CH₂Cl₂; acetonitrile / -15 °C

With 1H-imidazole; triethylsilane; 9-borabicyclo[3.3.1]nonane dimer; chloro-trimethyl-silane; N-methyl-2-indolinone; tetrapropylammonium perruthennate; methanesulfonamide; 4 A molecular sieve; thexylborane; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; potassium tert-butylate; hydrogen; iodine; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol; 9.1: Suzuki-Miyaura coupling / 9.2: Suzuki-Miyaura coupling;
DOI:10.1016/j.tetlet.2004.04.083

Reference yield:

: 725253-39-4
(3aS,4aS,6R,7R,8R,8aS,10aR)-7,8-Bis-benzyloxy-6-benzyloxymethyl-2,2-dimethyl-octahydro-1,3,5,9-tetraoxa-benzo[f]azulene

: 725253-52-1
C₄₆H₅₆O₁₀

Guidance literature:: Multi-step reaction with 13 steps

1.1: H₂ / Pd/C / ethyl acetate; methanol / 20 °C

2.1: CSA / CH₂Cl₂ / 20 °C

3.1: 92 percent / KOt-Bu; n-Bu₄NI / tetrahydrofuran / 20 °C

4.1: 100 percent / DIBAL-H / CH₂Cl₂ / -78 - 0 °C

5.1: 92 percent / I₂; PPh₃; imidazole / tetrahydrofuran / 20 °C

6.1: 99 percent / NaH / dimethylformamide / 0 - 20 °C

7.1: 9-BBN / tetrahydrofuran / 20 °C

7.2: aq. Cs₂CO₃ / PdCl₂(dppf)*CH₂Cl₂ / tetrahydrofuran; dimethylformamide / 50 °C

8.1: thexylborane / tetrahydrofuran / 0 °C

8.2: 78 percent / aq. NaOH; aq. H₂O₂ / tetrahydrofuran / 20 °C

9.1: TPAP; NMO; 4 Angstroem molecular sieves / CH₂Cl₂ / 20 °C

10.1: TMSCl; LiHMDS; Et₃N / tetrahydrofuran / -78 °C

10.2: Pd(OAc)2 / acetonitrile / 20 °C

11.1: 85 percent / DDQ / CH₂Cl₂ / 20 °C / pH 7

12.1: PPTS / toluene / 50 °C

13.1: Et₃SiH; BF₃*OEt₂ / CH₂Cl₂; acetonitrile / -15 °C

With 1H-imidazole; triethylsilane; 9-borabicyclo[3.3.1]nonane dimer; chloro-trimethyl-silane; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; thexylborane; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; potassium tert-butylate; hydrogen; iodine; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; triethylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; 7.1: Suzuki-Miyaura coupling / 7.2: Suzuki-Miyaura coupling;
DOI:10.1016/j.tetlet.2004.04.083