phenyl 4-(phenylseleno)(4,4-D₂)butyl sulfide

Base Information

• Chemical Name: phenyl 4-(phenylseleno)(4,4-D₂)butyl sulfide
• CAS No.: 140652-92-2
• Molecular Formula: C₁₆H₁₈SSe
• Molecular Weight: 323.329
• Mol file: 140652-92-2.mol

Synonyms:

Chemical Property of phenyl 4-(phenylseleno)(4,4-D₂)butyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl 4-(phenylseleno)(4,4-D₂)butyl sulfide

There total 4 articles about phenyl 4-(phenylseleno)(4,4-D₂)butyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 4-(phenylthio)butanoate (29193-72-4) → phenyl 4-(phenylseleno)(4,4-D2)butyl sulfide (140652-92-2)

Guidance literature:

Multi-step reaction with 3 steps

1: LiAlD₄ / diethyl ether

3: NaBH₄ / ethanol

With sodium tetrahydroborate; lithium aluminium deuteride; In diethyl ether; ethanol;

DOI:10.1071/CH9920475

Reference yield:

thiophenol (108-98-5) → phenyl 4-(phenylseleno)(4,4-D2)butyl sulfide (140652-92-2)

Guidance literature:

Multi-step reaction with 4 steps

1: NaH / dimethylformamide

2: LiAlD₄ / diethyl ether

4: NaBH₄ / ethanol

With sodium tetrahydroborate; lithium aluminium deuteride; sodium hydride; In diethyl ether; ethanol; N,N-dimethyl-formamide;

DOI:10.1071/CH9920475

Reference yield:

4-(phenylthio)(1,1-D2)butan-1-ol (140652-91-1) → phenyl 4-(phenylseleno)(4,4-D2)butyl sulfide (140652-92-2)

Guidance literature:

Multi-step reaction with 2 steps

2: NaBH₄ / ethanol

With sodium tetrahydroborate; In ethanol;

DOI:10.1071/CH9920475

upstream raw materials:

diphenyl diselenide

1,1-dideuterio-4-(phenylthio)butyl p-toluenesulfonate

ethyl 4-(phenylthio)butanoate

thiophenol

Downstream raw materials:

(1,1-D₂)butyl phenyl sulfide

(4,4-D₂)butyl phenyl sulfide