N,N-(dimethylamino)-S-phenyl-S-dichlorofluoromethyloxosulfonium tetrafluoroborate

Base Information

• Chemical Name: N,N-(dimethylamino)-S-phenyl-S-dichlorofluoromethyloxosulfonium tetrafluoroborate
• CAS No.: 1334160-40-5
• Molecular Formula: BF₄*C₉H₁₁Cl₂FNOS
• Molecular Weight: 357.967

Synonyms:

Chemical Property of N,N-(dimethylamino)-S-phenyl-S-dichlorofluoromethyloxosulfonium tetrafluoroborate

Chemical Property:

Purity/Quality:

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Technology Process of N,N-(dimethylamino)-S-phenyl-S-dichlorofluoromethyloxosulfonium tetrafluoroborate

There total 5 articles about N,N-(dimethylamino)-S-phenyl-S-dichlorofluoromethyloxosulfonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

CF3O3S(1-)*C9H11Cl2FNOS(1+) (1334160-38-1) → N,N-(dimethylamino)-S-phenyl-S-dichlorofluoromethyloxosulfonium tetrafluoroborate (1334160-40-5)

Guidance literature:

With sodium tetrafluoroborate; In methanol; water; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1002/ejoc.201100503

Reference yield:

N-(acetyl) dichlorofluoromethyl phenyl sulfilimine (1260111-81-6) → N,N-(dimethylamino)-S-phenyl-S-dichlorofluoromethyloxosulfonium tetrafluoroborate (1334160-40-5)

Guidance literature:

Multi-step reaction with 4 steps

1: hydrogenchloride; potassium permanganate / water / 1 h / 120 °C / Inert atmosphere

2: potassium carbonate / tetrahydrofuran / 18 h / Reflux; Inert atmosphere

3: 18 h / 20 °C / Inert atmosphere; Neat (no solvent)

4: sodium tetrafluoroborate / methanol; water / 18 h / 20 °C / Inert atmosphere

With hydrogenchloride; potassium permanganate; sodium tetrafluoroborate; potassium carbonate; In tetrahydrofuran; methanol; water;

DOI:10.1002/ejoc.201100503

Reference yield:

N-(acetyl) dichlorofluoromethyl phenyl sulfoximine (1334160-28-9) → N,N-(dimethylamino)-S-phenyl-S-dichlorofluoromethyloxosulfonium tetrafluoroborate (1334160-40-5)

Guidance literature:

Multi-step reaction with 4 steps

1: hydrogenchloride / water; acetonitrile / 18 h / 20 °C / Inert atmosphere

2: potassium carbonate / tetrahydrofuran / 18 h / Reflux; Inert atmosphere

3: 18 h / 20 °C / Inert atmosphere; Neat (no solvent)

4: sodium tetrafluoroborate / methanol; water / 18 h / 20 °C / Inert atmosphere

With hydrogenchloride; sodium tetrafluoroborate; potassium carbonate; In tetrahydrofuran; methanol; water; acetonitrile;

DOI:10.1002/ejoc.201100503

upstream raw materials:

N-(acetyl) dichlorofluoromethyl phenyl sulfilimine

(dichlorofluoromethyl)(imino)(phenyl)-λ⁶-sulfanone

N-methyl-S-phenyl-S-dichlorofluoromethylsulfoximine

CF₃O₃S^(1-)*C₉H₁₁Cl₂FNOS⁽¹⁺⁾

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