C₁₃H₁₀N₂O

Base Information

Chemical Name:C₁₃H₁₀N₂O
CAS No.:70357-61-8
Molecular Formula:C₁₃H₁₀N₂O
Molecular Weight:210.235
Hs Code.:

C<sub>13</sub>H<sub>10</sub>N<sub>2</sub>O

Synonyms:

Suppliers and Price of C₁₃H₁₀N₂O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₀N₂O

Chemical Property:

Purity/Quality:

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Technology Process of C₁₃H₁₀N₂O

There total 1 articles about C₁₃H₁₀N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 591-50-4
iodobenzene

: 70357-66-3
1H-pyrrolo[3,2-c]pyridine-6-ol

: 70357-61-8
C₁₃H₁₀N₂O

Guidance literature:: With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane; In 1,4-dioxane; at 110 ℃;
DOI:10.1016/j.bmcl.2011.06.112

Reference yield:

: 70357-61-8
C₁₃H₁₀N₂O

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: C₁₄H₉ClN₂O₂

Guidance literature:: C₁₃H₁₀N₂O; With bromine; In water; tert-butyl alcohol; at 20 ℃;

With palladium on activated charcoal; hydrogen; In ethanol; at 20 ℃;

N,N-dimethyl-formamide; Further stages;
DOI:10.1016/j.bmcl.2011.06.112

Reference yield:

: 70357-61-8
C₁₃H₁₀N₂O

: C₃₀H₃₁FN₄O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: bromine / water; tert-butyl alcohol / 20 °C

1.2: 20 °C

2.1: sodium dihydrogenphosphate; sodium chlorite / tert-butyl alcohol / 20 °C

3.1: 4-methyl-morpholine; O-<[cyano(ethoxycarbonyl)methylene]amino>-1,1,3,3-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 20 °C

4.1: 1-methyl-pyrrolidin-2-one; sodium hydride / 20 - 140 °C / Microwave irradiation

With 4-methyl-morpholine; 1-methyl-pyrrolidin-2-one; sodium chlorite; sodium dihydrogenphosphate; O-<[cyano(ethoxycarbonyl)methylene]amino>-1,1,3,3-tetramethyluronium tetrafluoroborate; bromine; sodium hydride; In water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: Vilsmeier-Haack formylation;
DOI:10.1016/j.bmcl.2011.06.112