Technology Process of C38H54N6O8
There total 4 articles about C38H54N6O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1-hydroxybenzotriazol-hydrate; triethylamine / dimethyl sulfoxide / 1.5 h / 20 °C
2: dimethyl sulfoxide
3: trifluoroacetic acid / dichloromethane / 3 h
With
1-hydroxybenzotriazol-hydrate; triethylamine; trifluoroacetic acid;
In
dichloromethane; dimethyl sulfoxide;
DOI:10.1039/c2sm26442k
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
for 3h;
DOI:10.1039/c2sm26442k
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / dichloromethane / 12 h / 0 - 20 °C
2: water; sodium hydroxide / methanol / 24 h / 0 - 20 °C
3: 1-hydroxybenzotriazol-hydrate; triethylamine / dimethyl sulfoxide / 1.5 h / 20 °C
4: dimethyl sulfoxide
5: trifluoroacetic acid / dichloromethane / 3 h
With
water; 1-hydroxybenzotriazol-hydrate; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1039/c2sm26442k