O⁴-methyl-N-phenyl-β-D-galactopyranosylamine

Base Information

• Chemical Name: O⁴-methyl-N-phenyl-β-D-galactopyranosylamine
• CAS No.: 17049-13-7
• Molecular Formula: C₁₃H₁₉NO₅
• Molecular Weight: 269.298
• Mol file: 17049-13-7.mol

Synonyms:

Chemical Property of O⁴-methyl-N-phenyl-β-D-galactopyranosylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O⁴-methyl-N-phenyl-β-D-galactopyranosylamine

There total 5 articles about O⁴-methyl-N-phenyl-β-D-galactopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

O4-Methyl-1,6;2,3-dianhydro-β-D-talopyranose (6893-60-3) → O4-methyl-N-phenyl-β-D-galactopyranosylamine (17049-13-7)

Guidance literature:

Multi-step reaction with 4 steps

1: diluted aqueous KOH-solution / Behandeln des Reaktionsprodukts mit Acetanhydrid und Pyridin

2: barium methylate; methanol

3: aqueous sulfuric acid

With methanol; potassium hydroxide; sulfuric acid; barium methoxide;

DOI:10.1021/ja01651a024

Reference yield:

O2,O3-Diacetyl-O4-methyl-1,6-anhydro-β-D-galactopyranose (95239-43-3) → O4-methyl-N-phenyl-β-D-galactopyranosylamine (17049-13-7)

Guidance literature:

Multi-step reaction with 3 steps

1: barium methylate; methanol

2: aqueous sulfuric acid

With methanol; sulfuric acid; barium methoxide;

DOI:10.1021/ja01651a024

Reference yield:

O4-Methyl-1,6-anhydro-β-D-galactopyranose (98155-09-0) → O4-methyl-N-phenyl-β-D-galactopyranosylamine (17049-13-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous sulfuric acid

With sulfuric acid;

DOI:10.1021/ja01651a024

upstream raw materials:

4-O-methyl-galactose

O⁴-Methyl-1,6;2,3-dianhydro-β-D-talopyranose

O²,O³-Diacetyl-O⁴-methyl-1,6-anhydro-β-D-galactopyranose

O⁴-Methyl-1,6-anhydro-β-D-galactopyranose