Technology Process of C52H56N4O8S
There total 6 articles about C52H56N4O8S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide; acetic acid / water / 120 °C / Sealed tube; Microwave irradiation
2: tetrakis(triphenylphosphine) palladium(0); phenylsilane / dichloromethane / 0.17 h / 20 °C / Inert atmosphere
3: dichloromethane / 1 h / 20 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); phenylsilane; acetic acid; potassium hydroxide;
In
dichloromethane; water;
DOI:10.1021/ja311961k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0); phenylsilane / dichloromethane / 0.17 h / 20 °C / Inert atmosphere
2: dichloromethane / 1 h / 20 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); phenylsilane;
In
dichloromethane;
DOI:10.1021/ja311961k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / water; 1,4-dioxane / 0 - 20 °C / pH 9
2: dicyclohexyl-carbodiimide / ethyl acetate / 20 °C
3: dichloromethane / 1 h / 20 °C / Inert atmosphere
With
dicyclohexyl-carbodiimide; sodium hydroxide;
In
1,4-dioxane; dichloromethane; water; ethyl acetate;
DOI:10.1021/ja311961k