C₁₁H₁₃F₃O₂

Base Information

• Chemical Name: C₁₁H₁₃F₃O₂
• CAS No.: 1380436-39-4
• Molecular Formula: C₁₁H₁₃F₃O₂
• Molecular Weight: 234.218
• Mol file: 1380436-39-4.mol

Synonyms:

Chemical Property of C₁₁H₁₃F₃O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₁H₁₃F₃O₂

There total 2 articles about C₁₁H₁₃F₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C34H47BO → C11H13F3O2 (1380436-39-4) + C11H13F3O2 (1380436-35-0)

Guidance literature:

C₃₄H₄₇BO; With borane-THF; In diethyl ether; pentane; at 20 ℃; for 0.0833333h; Inert atmosphere;

With dihydrogen peroxide; In diethyl ether; pentane; at 0 - 20 ℃; for 4h; Inert atmosphere; Alkaline conditions;

DOI:10.1021/jo300414u

Reference yield:

1-naphthaldehyde (66-77-3) → C11H13F3O2 (1380436-39-4) + C11H13F3O2 (1380436-35-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: diethyl ether; pentane / 0.08 h / -100 °C / Inert atmosphere

2.1: borane-THF / diethyl ether; pentane / 0.08 h / 20 °C / Inert atmosphere

2.2: 4 h / 0 - 20 °C / Inert atmosphere; Alkaline conditions

With borane-THF; In diethyl ether; pentane;

DOI:10.1021/jo300414u

upstream raw materials:

1-naphthaldehyde