tert-butyl 5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2,4-dideoxy-2-methyl-D-erythropentonate

Base Information

Chemical Name:tert-butyl 5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2,4-dideoxy-2-methyl-D-erythropentonate
CAS No.:1448551-47-0
Molecular Formula:C₃₁H₃₈O₆
Molecular Weight:506.639
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2,4-dideoxy-2-methyl-D-erythropentonate

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Technology Process of tert-butyl 5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2,4-dideoxy-2-methyl-D-erythropentonate

There total 2 articles about tert-butyl 5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2,4-dideoxy-2-methyl-D-erythropentonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428671-95-7
C₂₄H₂₄O₄

: C₂₇H₄₇BO₂

: 1448551-47-0
tert-butyl 5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2,4-dideoxy-2-methyl-D-erythropentonate

: tert-butyl 5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2,4-dideoxy-2-methylpentonate

Guidance literature:: C₂₄H₂₄O₄; C₂₇H₄₇BO₂; In diethyl ether; at -78 ℃; for 12h; Inert atmosphere;

With dihydrogen peroxide; In methanol; diethyl ether; at 20 ℃; for 6h; Overall yield = 77 %; Overall yield = 40 mg; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol401679g

Reference yield:

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 1448551-47-0
tert-butyl 5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2,4-dideoxy-2-methyl-D-erythropentonate

: tert-butyl 5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2,4-dideoxy-2-methylpentonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether / 2 h / 0 °C / Inert atmosphere

2.1: diethyl ether / 12 h / -78 °C / Inert atmosphere

2.2: 3407 / 6 h / 20 °C / Inert atmosphere

In diethyl ether;
DOI:10.1021/ol401679g