C₃₁H₄₁N₃O₄

Base Information

Chemical Name:C₃₁H₄₁N₃O₄
CAS No.:1089704-76-6
Molecular Formula:C₃₁H₄₁N₃O₄
Molecular Weight:519.684
Hs Code.:

C<sub>31</sub>H<sub>41</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₃₁H₄₁N₃O₄

Chemical Property:

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Technology Process of C₃₁H₄₁N₃O₄

There total 15 articles about C₃₁H₄₁N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1373756-53-6
(2R,3S)-3-amino-4-(4-ethynylphenyl)-1-((S)-6′-neopentyl-3′,4′-dihydrospiro[cyclobutane-1,2′-pyrano[2,3-b]pyridine]-4′-ylamino)butan-2-ol

: 31059-08-2
1-(1H-imidazol-1-yl)-2-methoxyethanone

: 1089704-76-6
C₃₁H₄₁N₃O₄

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jm300118s

Reference yield:

: 1-(prop-2-en-1-yl)cyclobutanol

: 1089704-76-6
C₃₁H₄₁N₃O₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: triethylamine / dichloromethane / 0.5 h / Cooling with ice

2.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 2 h / 20 °C

3.1: sodium periodate / tetrahydrofuran; water; tert-butyl alcohol / 1.5 h

4.1: copper(II) sulfate / dichloromethane / 16 h / 20 °C

5.1: n-butyllithium; 2,2,6,6-tetramethyl-piperidine / tetrahydrofuran; toluene / 0.5 h / 0 °C

5.2: 0.5 h / -65 - -10 °C

6.1: cesium fluoride / dimethyl sulfoxide / 15 h / 120 °C

7.1: hydrogenchloride / dichloromethane / 1 h / 25 °C

8.1: trimethyl orthoformate; sodium tris(acetoxy)borohydride / dichloromethane / 2 h / 23 °C

9.1: XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / tetrahydrofuran / 0.25 h / Inert atmosphere

9.2: 0.67 h / 135 °C / Inert atmosphere; Microwave irradiation

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h

11.1: hydrogenchloride / 1,4-dioxane; methanol / 1 h / 50 °C

12.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

With 2,2,6,6-tetramethyl-piperidine; hydrogenchloride; sodium periodate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; osmium(VIII) oxide; n-butyllithium; tetrabutyl ammonium fluoride; sodium tris(acetoxy)borohydride; copper(II) sulfate; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; cesium fluoride; XPhos; trimethyl orthoformate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; dimethyl sulfoxide; toluene; tert-butyl alcohol;
DOI:10.1021/jm300118s

Reference yield:

: 939411-88-8
3-(1-(tert-butyldimethylsilyloxy)cyclobutyl)propane-1,2-diol

: 1089704-76-6
C₃₁H₄₁N₃O₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium periodate / tetrahydrofuran; water; tert-butyl alcohol / 1.5 h

2.1: copper(II) sulfate / dichloromethane / 16 h / 20 °C

3.1: n-butyllithium; 2,2,6,6-tetramethyl-piperidine / tetrahydrofuran; toluene / 0.5 h / 0 °C

3.2: 0.5 h / -65 - -10 °C

4.1: cesium fluoride / dimethyl sulfoxide / 15 h / 120 °C

5.1: hydrogenchloride / dichloromethane / 1 h / 25 °C

6.1: trimethyl orthoformate; sodium tris(acetoxy)borohydride / dichloromethane / 2 h / 23 °C

7.1: XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / tetrahydrofuran / 0.25 h / Inert atmosphere

7.2: 0.67 h / 135 °C / Inert atmosphere; Microwave irradiation

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h

9.1: hydrogenchloride / 1,4-dioxane; methanol / 1 h / 50 °C

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

With 2,2,6,6-tetramethyl-piperidine; hydrogenchloride; sodium periodate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; n-butyllithium; tetrabutyl ammonium fluoride; sodium tris(acetoxy)borohydride; copper(II) sulfate; N-ethyl-N,N-diisopropylamine; cesium fluoride; XPhos; trimethyl orthoformate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; dimethyl sulfoxide; toluene; tert-butyl alcohol;
DOI:10.1021/jm300118s